30-Hydroxytriacontanoic acid

Base Information Edit

Chemical Name:30-Hydroxytriacontanoic acid
CAS No.:52900-18-2
Molecular Formula:C30H60O3
Molecular Weight:468.805
Hs Code.:
DSSTox Substance ID:DTXSID40415598
Nikkaji Number:J1.723.548F
Wikidata:Q27145817
Metabolomics Workbench ID:1416
Mol file:52900-18-2.mol

Synonyms:30-hydroxytriacontanoic acid;30-hydroxy-triacontanoic acid;omega-hydroxytriacontanoic acid;52900-18-2;30-hydroxymelissic acid;omega-hydroxymelissic acid;SCHEMBL1948521;CHEBI:76220;DTXSID40415598;LMFA01050221;Q27145817

Suppliers and Price of 30-Hydroxytriacontanoic acid

Supply Marketing:Edit

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of 30-Hydroxytriacontanoic acid Edit

Chemical Property:

XLogP3:11.8
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:29
Exact Mass:468.45424577
Heavy Atom Count:33
Complexity:370

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C(CCCCCCCCCCCCCCC(=O)O)CCCCCCCCCCCCCCO

Technology Process of 30-Hydroxytriacontanoic acid

There total 13 articles about 30-Hydroxytriacontanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 79162-70-2
methyl 30-hydroxytriacontanoate

: 52900-18-2
30-hydroxytriacontanoic acid

Guidance literature:: With sodium hydroxide; In methanol; for 24h; Heating;

Reference yield:

: 37935-47-0
2-(5-bromopentyloxy)tetrahydropyran

: 52900-18-2
30-hydroxytriacontanoic acid

Guidance literature:: Multi-step reaction with 7 steps

1.1: Mg / tetrahydrofuran

1.2: 95 percent / MeMgCl; Li₂CuCl₄ / tetrahydrofuran / 16 h / -20 - 20 °C

2.1: 77 percent / pyridinium chlorochromate / CH₂Cl₂ / 2.5 h / 20 °C

3.1: (Me₃Si)2NNa / tetrahydrofuran / 1.5 h

3.2: tetrahydrofuran / 16 h / -20 - 20 °C

4.1: 42.86 g / diethyl ether

5.1: H₂ / 10 percent Pd/C / ethyl acetate

6.1: TsOH / methanol / 20 °C

7.1: 95 percent / NaOH / methanol / 24 h / Heating

With sodium hydroxide; hydrogen; sodium hexamethyldisilazane; toluene-4-sulfonic acid; magnesium; pyridinium chlorochromate; palladium on activated charcoal; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; ethyl acetate; 3.2: Wittig reaction;

Reference yield:

: 111-29-5
1 ,5-pentanediol

: 52900-18-2
30-hydroxytriacontanoic acid

Guidance literature:: Multi-step reaction with 9 steps

1.1: 36 percent / aq. HBr / 22 h / 80 °C

2.1: 96 percent / conc. HCl / 2.5 h / 20 °C

3.1: Mg / tetrahydrofuran

3.2: 95 percent / MeMgCl; Li₂CuCl₄ / tetrahydrofuran / 16 h / -20 - 20 °C

4.1: 77 percent / pyridinium chlorochromate / CH₂Cl₂ / 2.5 h / 20 °C

5.1: (Me₃Si)2NNa / tetrahydrofuran / 1.5 h

5.2: tetrahydrofuran / 16 h / -20 - 20 °C

6.1: 42.86 g / diethyl ether

7.1: H₂ / 10 percent Pd/C / ethyl acetate

8.1: TsOH / methanol / 20 °C

9.1: 95 percent / NaOH / methanol / 24 h / Heating

With hydrogenchloride; sodium hydroxide; hydrogen bromide; hydrogen; sodium hexamethyldisilazane; toluene-4-sulfonic acid; magnesium; pyridinium chlorochromate; palladium on activated charcoal; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; ethyl acetate; 5.2: Wittig reaction;