3-Acetoxycyclohexanone

Base Information

Chemical Name:3-Acetoxycyclohexanone
CAS No.:53164-77-5
Molecular Formula:C8H12O3
Molecular Weight:156.181
Hs Code.:
DSSTox Substance ID:DTXSID80549583
Nikkaji Number:J2.984.346E
Mol file:53164-77-5.mol

Synonyms:3-Acetoxycyclohexanone;53164-77-5;3-Oxocyclohexyl acetate;SCHEMBL8805010;DTXSID80549583

Suppliers and Price of 3-Acetoxycyclohexanone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 0 raw suppliers

Chemical Property of 3-Acetoxycyclohexanone

Chemical Property:

XLogP3:0.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:2
Exact Mass:156.078644241
Heavy Atom Count:11
Complexity:174

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(=O)OC1CCCC(=O)C1

Technology Process of 3-Acetoxycyclohexanone

There total 4 articles about 3-Acetoxycyclohexanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 823-19-8
3-hydroxycyclohexanone

: 108-24-7
acetic anhydride

: 53164-77-5
3-oxocyclohexyl acetate

Guidance literature:: With pyridine; at 20 ℃; for 12h;
DOI:10.1016/j.tetasy.2011.09.011

Reference yield:

: 622-45-7
cyclohexyl acetate

: 53164-77-5
3-oxocyclohexyl acetate

: 41043-88-3
4-acetoxycyclohexanone

Guidance literature:: With tert.-butylhydroperoxide; [bis(acetoxy)iodo]benzene; In water; acetonitrile; at 25 ℃; for 2h;
DOI:10.1021/ol2016466

Reference yield:

: 504-01-8
cyclohexane-1,3-diol

: 53164-77-5
3-oxocyclohexyl acetate

Guidance literature:: Multi-step reaction with 2 steps

1: chloroform

2: benzene; aqueous acetic acid; CrO₃ / 50 °C

With chromium(VI) oxide; chloroform; acetic acid; benzene;