9-Methoxy-2,6,8-trimethyl-4H-pyrrolo(3,2,1-ij)quinolin-4-one

Base Information

Chemical Name:9-Methoxy-2,6,8-trimethyl-4H-pyrrolo(3,2,1-ij)quinolin-4-one
CAS No.:131195-85-2
Molecular Formula:C₁₅H₁₅NO₂
Molecular Weight:241.29
Hs Code.:
DSSTox Substance ID:DTXSID80156953
Nikkaji Number:J374.645C

Synonyms:9-Methoxy-2,6,8-trimethyl-4H-pyrrolo(3,2,1-ij)quinolin-4-one;131195-85-2;DTXSID80156953

Suppliers and Price of 9-Methoxy-2,6,8-trimethyl-4H-pyrrolo(3,2,1-ij)quinolin-4-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemicals and raw materials
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Total 1 raw suppliers

Chemical Property of 9-Methoxy-2,6,8-trimethyl-4H-pyrrolo(3,2,1-ij)quinolin-4-one

Chemical Property:

Vapor Pressure:0.000698mmHg at 25°C
Boiling Point:308°Cat760mmHg
Flash Point:140.1°C
Density:1.2g/cm³
XLogP3:2.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:241.110278721
Heavy Atom Count:18
Complexity:403

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC2=C3C(=C1OC)C=C(N3C(=O)C=C2C)C

Technology Process of 9-Methoxy-2,6,8-trimethyl-4H-pyrrolo(3,2,1-ij)quinolin-4-one

There total 11 articles about 9-Methoxy-2,6,8-trimethyl-4H-pyrrolo(3,2,1-ij)quinolin-4-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 131195-82-9
2,6,8-trimethyl-9-hydroxypyrrolo<3,2,1-ij>quinolin-4-one

: 77-78-1
dimethyl sulfate

: 131195-85-2
2,6,8-trimethyl-9-methoxypyrrolo<3,2,1-ij>quinolin-4-one

Guidance literature:: With potassium carbonate; In acetone; Heating;
DOI:10.1021/jo00003a016

Reference yield: 65.0%

: 159838-19-4
9-Methoxy-2,6,8-trimethyl-1,2-dihydro-pyrrolo[3,2,1-ij]quinolin-4-one

: 131195-85-2
2,6,8-trimethyl-9-methoxypyrrolo<3,2,1-ij>quinolin-4-one

Guidance literature:: With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In toluene; for 1h; Heating;

Reference yield:

: 131195-74-9
4,6-dimethyl-7-hydroxy-8-allylquinolin-2-one

: 131195-85-2
2,6,8-trimethyl-9-methoxypyrrolo<3,2,1-ij>quinolin-4-one

Guidance literature:: Multi-step reaction with 4 steps

1: 88 percent / K₂CO₃ / acetone / 1 h / Heating

2: 21 percent / HI (57percent) / acetic acid / 20 h / 65 °C

3: 53 percent / 4percent KOH / ethanol / 0.5 h / Ambient temperature

4: 65 percent / 2,3-dichloro-5,6-dicyanobenzoquinone / toluene / 1 h / Heating

With potassium hydroxide; hydrogen iodide; potassium carbonate; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In ethanol; acetic acid; acetone; toluene;