Hydrazinecarbothioamide, 2-(1-methyl-2-oxopropylidene)-N-phenyl-

Base Information

Chemical Name:Hydrazinecarbothioamide, 2-(1-methyl-2-oxopropylidene)-N-phenyl-
CAS No.:53534-12-6
Molecular Formula:C₁₁H₁₃N₃OS
Molecular Weight:235.31
Hs Code.:
DSSTox Substance ID:DTXSID80399388
Mol file:53534-12-6.mol

Synonyms:53534-12-6;Hydrazinecarbothioamide, 2-(1-methyl-2-oxopropylidene)-N-phenyl-;SCHEMBL1641570;DTXSID80399388

Suppliers and Price of Hydrazinecarbothioamide, 2-(1-methyl-2-oxopropylidene)-N-phenyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of Hydrazinecarbothioamide, 2-(1-methyl-2-oxopropylidene)-N-phenyl-

Chemical Property:

XLogP3:1.9
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:3
Exact Mass:235.07793322
Heavy Atom Count:16
Complexity:296

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(=NNC(=S)NC1=CC=CC=C1)C(=O)C

Technology Process of Hydrazinecarbothioamide, 2-(1-methyl-2-oxopropylidene)-N-phenyl-

There total 1 articles about Hydrazinecarbothioamide, 2-(1-methyl-2-oxopropylidene)-N-phenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 431-03-8
dimethylglyoxal

: 5351-69-9
4-Phenyl-3-thiosemicarbazide

: 149096-44-6,53534-12-6
biacetyl (4-phenyl)-thiosemicarbazone

Guidance literature:: With hydrogenchloride; In water; at 10 ℃; for 1.5h; Cooling with ice;
DOI:10.1039/c2dt12096h

Reference yield: 76.0%

: 6926-58-5
4,4-dimethylthiosemicarbazide

: 5970-45-6
zinc(II) acetate dihydrate

: 149096-44-6,53534-12-6
biacetyl (4-phenyl)-thiosemicarbazone

: [(CH₃)2NC(S)NNC(CH₃)C(CH₃)NNC(S)NHC₆H₅]Zn

Guidance literature:: With glacial acetic acid; triethylamine; In tetrahydrofuran; methanol; thiosemicarbazide-compound in THF was treated with glacial CH3COOH for ca. 20 min, carbonyl-compound was added, stirred at room temp. for 3 h, Zn-compound in methanol was added followed by N(C2H5)3, stirred overnightat room temp.; evapd., suspd. in methanol, the solid was filtered off, washed with methanol, dried in vac.;
DOI:10.1039/c2dt12096h