2-Bromo-6-methylbenzoyl chloride

Base Information

Chemical Name:2-Bromo-6-methylbenzoyl chloride
CAS No.:535961-79-6
Molecular Formula:C8H6BrClO
Molecular Weight:233.492
Hs Code.:
DSSTox Substance ID:DTXSID101302296
Mol file:535961-79-6.mol

Synonyms:2-Bromo-6-methylbenzoyl chloride;535961-79-6;SCHEMBL7539855;2-Bromo-6-methylbenzoylchloride;DTXSID101302296;DA-05121

Suppliers and Price of 2-Bromo-6-methylbenzoyl chloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 2-Bromo-6-methylbenzoyl chloride

Chemical Property:

XLogP3:3.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:1
Exact Mass:231.92906
Heavy Atom Count:11
Complexity:160

Purity/Quality:: 95% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=C(C(=CC=C1)Br)C(=O)Cl

Technology Process of 2-Bromo-6-methylbenzoyl chloride

There total 1 articles about 2-Bromo-6-methylbenzoyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4389-50-8
2-amino-6-methylbenzoic acid

: 535961-79-6
2-bromo-6-methylbenzoyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1: 65 percent / CuBr, aq. HBr, NaNO₂ / 1) 90 deg C, 1 h, 2) reflux, 0.5 h, 3) RT, 2 h

2: oxalyl chloride / CH₂Cl₂ / 24 h / Ambient temperature

With oxalyl dichloride; hydrogen bromide; copper(I) bromide; sodium nitrite; In dichloromethane;
DOI:10.1021/jo00064a017