Chromium,pentacarbonyl[thiobis[methane]]-, (OC-6-22)- (9CI)

Base Information

Chemical Name:Chromium,pentacarbonyl[thiobis[methane]]-, (OC-6-22)- (9CI)
CAS No.:31172-83-5
Molecular Formula:C₇H₆CrO₅S
Molecular Weight:254.184
Hs Code.:

Synonyms:Chromium,pentacarbonyl(methyl sulfide)- (8CI); Pentacarbonyl(dimethyl sulfide)chromium

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Chemical Property of Chromium,pentacarbonyl[thiobis[methane]]-, (OC-6-22)- (9CI)

Chemical Property:

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MSDS Files:: SDS file from LookChem

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Technology Process of Chromium,pentacarbonyl[thiobis[methane]]-, (OC-6-22)- (9CI)

There total 1 articles about Chromium,pentacarbonyl[thiobis[methane]]-, (OC-6-22)- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 29892-37-3
chloro(dimethylsulfide) gold(I)

: (1,2-dimethyl-5-phenylpyridin-4(1H)-ylidene)pentacarbonylchromium

: 2926-30-9
sodium triflate

: 603-35-0
triphenylphosphine

: 31172-83-5
((CH₃)2S)pentacarbonylchromium

: (1,2-dimethyl-5-phenylpyridin-4(1H)-ylidene)(triphenylphosphane)gold(I) triflate

Guidance literature:: In acetonitrile; (Ar), Au complex and PPh3 (1:1) mixed in CH3CN, suspn. stirred at room temp. for 45 min, cooled to -45°C, treated over 10 min with solid NaOTf, treated with Cr complex in CH3CN, cooled to -45°C, stirredat room temp. for 4 h; evapd.(vac.), dissolved (CH2Cl2), filtered, evapd., extd.(toluene), crystd.(CH2Cl2)/pentane), elem. anal.;
DOI:10.1002/ejic.200801180