4-Methoxy-N-(1,2,2,2-tetrachloroethyl)benzamide

Base Information

Chemical Name:4-Methoxy-N-(1,2,2,2-tetrachloroethyl)benzamide
CAS No.:53998-83-7
Molecular Formula:C10H9Cl4NO2
Molecular Weight:316.999
Hs Code.:
DSSTox Substance ID:DTXSID60492028
Nikkaji Number:J1.511.360J

Synonyms:53998-83-7;Benzamide, 4-methoxy-N-(1,2,2,2-tetrachloroethyl)-;4-Methoxy-N-(1,2,2,2-tetrachloroethyl)benzamide;DTXSID60492028

Suppliers and Price of 4-Methoxy-N-(1,2,2,2-tetrachloroethyl)benzamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-Methoxy-N-(1,2,2,2-tetrachloroethyl)benzamide

Chemical Property:

XLogP3:3.8
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:316.935789
Heavy Atom Count:17
Complexity:262

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=CC=C(C=C1)C(=O)NC(C(Cl)(Cl)Cl)Cl

Technology Process of 4-Methoxy-N-(1,2,2,2-tetrachloroethyl)benzamide

There total 2 articles about 4-Methoxy-N-(1,2,2,2-tetrachloroethyl)benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 63499-61-6
N-(2,2,2-trichloro-1-hydroxyethyl)-4-methoxybenzamide

: 53998-83-7
N-(1,2,2,2-tetrachloroethyl)-4-methoxybenzamide

Guidance literature:: With phosphorus pentachloride; In chloroform; at 20 ℃; for 0.5h;
DOI:10.1016/S0040-4020(01)00434-3

Reference yield:

: 3424-93-9
4-methoxyphenylacetamide

: 53998-83-7
N-(1,2,2,2-tetrachloroethyl)-4-methoxybenzamide

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / 90 - 100 °C

2: 95 percent / PCl₅ / CHCl₃ / 0.5 h / 20 °C

With phosphorus pentachloride; In chloroform;
DOI:10.1016/S0040-4020(01)00434-3

Reference yield: 98.0%

: 53998-83-7
N-(1,2,2,2-tetrachloroethyl)-4-methoxybenzamide

: 54888-29-8
N-(2,2-dichlorovinyl)-4-methoxybenzamide

Guidance literature:: With lithium perchlorate; In acetonitrile; at 15 ℃; Electrochemical reaction; cathode - mercury pool, anode - platinum plate, cathodic potential - 0.60 V vs SCE, electricity consumption - 2 F/mol;
DOI:10.1016/S0040-4020(01)00434-3