1,4-Benzenediamine, N,N-dimethyl-N'-[(4-nitrophenyl)methylene]-, (E)-

Base Information

Chemical Name:1,4-Benzenediamine, N,N-dimethyl-N'-[(4-nitrophenyl)methylene]-, (E)-
CAS No.:54050-72-5
Molecular Formula:C₁₅H₁₅N₃O₂
Molecular Weight:269.303
Hs Code.:

Synonyms:N,N-dimethyl-4-[(1E)-(4-nitrobenzylidene)amine]aniline;p-Dimethylamino-(p-nitrobenzyliden)-anilin;4-dimethylamino-N-(4-nitrobenzylidene)aniline;N,N-Dimethyl-N'-[1-(4-nitro-phenyl)-meth-(E)-ylidene]-benzene-1,4-diamine;p-Nitrobenzyliden-p-dimethylaminoanilin;

Suppliers and Price of 1,4-Benzenediamine, N,N-dimethyl-N'-[(4-nitrophenyl)methylene]-, (E)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,4-Benzenediamine, N,N-dimethyl-N'-[(4-nitrophenyl)methylene]-, (E)-

Chemical Property:

Melting Point:220 °C(Solv: xylene (1330-20-7))
Boiling Point:451.8±30.0 °C(Predicted)
PSA：61.42000
Density:1.14±0.1 g/cm3(Predicted)
LogP:3.93460

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1,4-Benzenediamine, N,N-dimethyl-N'-[(4-nitrophenyl)methylene]-, (E)-

There total 5 articles about 1,4-Benzenediamine, N,N-dimethyl-N'-[(4-nitrophenyl)methylene]-, (E)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.8%

: 555-16-8
4-nitrobenzaldehdye

: 99-98-9
4-amino-N,N-dimethylaniline

: 54050-72-5
N,N-dimethyl-N'-<(4-nitrophenyl)methylene>-1,4-benzenediamine

Guidance literature:: With acetic acid; In methanol; for 3h;
DOI:10.1002/poc.3402

Reference yield:

: 111955-89-6
N,N-dimethyl-N'-<(4-nitrophenyl)methylene>-1,4-benzenediamine

: 54050-72-5
N,N-dimethyl-N'-<(4-nitrophenyl)methylene>-1,4-benzenediamine

Guidance literature:: In hexane; at 25 ℃; under 750.06 Torr; Rate constant; Thermodynamic data; ΔV (excit.) var.pressure, solvent;
DOI:10.1021/jo00263a022

Reference yield:

: N,N-dimethyl-p-nitrosoaniline

: 54050-72-5
N,N-dimethyl-N'-<(4-nitrophenyl)methylene>-1,4-benzenediamine

Guidance literature:: Multi-step reaction with 2 steps

1: tin; hydrogenchloride / ethanol; water / Reflux

2: acetic acid / methanol / 3 h

With hydrogenchloride; tin; acetic acid; In methanol; ethanol; water;
DOI:10.1002/poc.3402