4-(3-Phenylprop-2-enoylamino)benzoic acid

Base Information

Chemical Name:4-(3-Phenylprop-2-enoylamino)benzoic acid
CAS No.:54057-59-9
Molecular Formula:C16H13NO3
Molecular Weight:267.27900
Hs Code.:2924299090
DSSTox Substance ID:DTXSID20354178
Mol file:54057-59-9.mol

Synonyms:4-(3-phenylprop-2-enoylamino)benzoic acid;Enamine_002316;SCHEMBL2848898;DTXSID20354178;AKOS030750137

Suppliers and Price of 4-(3-Phenylprop-2-enoylamino)benzoic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 9 raw suppliers

Chemical Property of 4-(3-Phenylprop-2-enoylamino)benzoic acid

Chemical Property:

Vapor Pressure:2.08E-12mmHg at 25°C
Boiling Point:538.1oC at 760 mmHg
Flash Point:279.2oC
PSA：66.40000
Density:1.31g/cm3
LogP:3.10970
XLogP3:3.1
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:4
Exact Mass:267.08954328
Heavy Atom Count:20
Complexity:364

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)C=CC(=O)NC2=CC=C(C=C2)C(=O)O

Technology Process of 4-(3-Phenylprop-2-enoylamino)benzoic acid

There total 3 articles about 4-(3-Phenylprop-2-enoylamino)benzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 102-92-1,17082-09-6
cinnamoyl chloride

: 150-13-0,159246-81-8,8014-65-1
4-amino-benzoic acid

: 54057-59-9
4-{[(2E)-3-phenylprop-2-enoyl]amino}benzoic acid

Guidance literature:: With pyridine; In toluene; for 12h;
DOI:10.1007/BF00777140

Reference yield: 97.0%

: 140-10-3
(E)-3-phenylacrylic acid

: 150-13-0,159246-81-8,8014-65-1
4-amino-benzoic acid

: 54057-59-9
4-{[(2E)-3-phenylprop-2-enoyl]amino}benzoic acid

Guidance literature:: With N,N-dimethyl-formamide; dicyclohexyl-carbodiimide; In neat (no solvent); at 140 ℃; for 0.025h; Microwave irradiation;
DOI:10.1080/00397911.2011.604148

Reference yield:

: 150-13-0,159246-81-8,8014-65-1
4-amino-benzoic acid

: 102-92-1,17082-09-6
Cinnamoyl chloride

: 54057-59-9
4-{[(2E)-3-phenylprop-2-enoyl]amino}benzoic acid

Guidance literature:: 4-amino-benzoic acid; With triethylamine; In dichloromethane; at 20 ℃; for 0.5h;

Cinnamoyl chloride; In dichloromethane; for 2h;
DOI:10.1248/cpb.60.385