2-Propyn-1-one, 1,1'-(1,2-phenylene)bis-

Base Information

Chemical Name:2-Propyn-1-one, 1,1'-(1,2-phenylene)bis-
CAS No.:54160-73-5
Molecular Formula:C12H6O2
Molecular Weight:182.178
Hs Code.:
DSSTox Substance ID:DTXSID30458292
Nikkaji Number:J1.912.069D
Wikidata:Q82281499

Synonyms:54160-73-5;1,1'-(1,2-Phenylene)bis(prop-2-yn-1-one);1,2-bis(propiolyl)benzene;2-Propyn-1-one, 1,1'-(1,2-phenylene)bis-;1,2-Dipropiolylbenzene;DTXSID30458292

Suppliers and Price of 2-Propyn-1-one, 1,1'-(1,2-phenylene)bis-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 0 raw suppliers

Chemical Property of 2-Propyn-1-one, 1,1'-(1,2-phenylene)bis-

Chemical Property:

XLogP3:2.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:182.036779430
Heavy Atom Count:14
Complexity:311

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C#CC(=O)C1=CC=CC=C1C(=O)C#C

Technology Process of 2-Propyn-1-one, 1,1'-(1,2-phenylene)bis-

There total 3 articles about 2-Propyn-1-one, 1,1'-(1,2-phenylene)bis- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 141068-38-4
1-[2-(1-hydroxy-prop-2-ynyl)-phenyl]-prop-2-yn-1-ol

: 54160-73-5
1,1'-(1,2-phenylene)bis(prop-2-yn-1-one)

Guidance literature:: With Dess-Martin periodane; In dichloromethane; at 0 ℃; for 1h; Schlenk technique; Inert atmosphere;
DOI:10.1002/anie.202006689

Reference yield:

: 643-79-8
o-phthalic dicarboxaldehyde

: 54160-73-5
1,1'-(1,2-phenylene)bis(prop-2-yn-1-one)

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran / 2 h / 60 °C / Schlenk technique; Inert atmosphere

2: Dess-Martin periodane / dichloromethane / 1 h / 0 °C / Schlenk technique; Inert atmosphere

With Dess-Martin periodane; In tetrahydrofuran; dichloromethane;
DOI:10.1002/anie.202006689