2,2,6,6-Tetramethylpiperidine-1-carbaldehyde

Base Information

• Chemical Name: 2,2,6,6-Tetramethylpiperidine-1-carbaldehyde
• CAS No.: 54262-97-4
• Molecular Formula: C10H19NO
• Molecular Weight: 169.267
• DSSTox Substance ID: DTXSID70535076
• Nikkaji Number: J3.471.531I
• Wikidata: Q82409174

Synonyms:2,2,6,6-Tetramethylpiperidine-1-carbaldehyde;54262-97-4;SCHEMBL5519734;DTXSID70535076

Chemical Property of 2,2,6,6-Tetramethylpiperidine-1-carbaldehyde

Chemical Property:

• XLogP3: 1.8
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 0
• Exact Mass: 169.146664230
• Heavy Atom Count: 12
• Complexity: 168

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC1(CCCC(N1C=O)(C)C)C

Technology Process of 2,2,6,6-Tetramethylpiperidine-1-carbaldehyde

There total 3 articles about 2,2,6,6-Tetramethylpiperidine-1-carbaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

1,2,2,6,6-pentamethylpiperidine (79-55-0) → 2,2,6,6-tetramethyl-piperidine (768-66-1) + 2,2,6,6-tetramethylpiperidine-1-carboxaldehyde (54262-97-4)

Guidance literature:

With ruthenium tetroxide; In tetrachloromethane; for 2h;

DOI:10.1002/ardp.19843170712

Reference yield: 41.0%

1,2,2,6,6-pentamethylpiperidine (79-55-0) → 2,2,6,6-tetramethyl-piperidine (768-66-1) + TEMPO (5132-07-0) + 2,2,6,6-tetramethylpiperidine-1-carboxaldehyde (54262-97-4)

Guidance literature:

With sodium periodate; ruthenium tetroxide; In tetrachloromethane; water; for 5h;

DOI:10.1002/ardp.19843170106

Reference yield: 23.0%

1-(bis((SS,SS)-p-tolylsulfinyl)methoxy)-2,2,6,6-tetramethylpiperidine → di(p-tolyl) disulfide (103-19-5) + di(4-methyl)phenylthiosulfonate (2943-42-2) + 2,2,6,6-tetramethylpiperidine-1-carboxaldehyde (54262-97-4) + N-(p-toluenesulphinyl)-2,2,6,6-tetramethylpiperidine

Guidance literature:

In benzene; at 100 ℃; for 17h; Sealed tube; Inert atmosphere; Darkness;

DOI:10.1071/CH12545

upstream raw materials:

1,2,2,6,6-pentamethylpiperidine

Downstream raw materials:

2,4,6-tris(4-methoxyphenyl)-2,4,6-trisulfanylene-1,3,5,2,4,6-trioxatriphosphinane

1-prop-2-yl-2-pyrrolecarboxaldehyde

1-isopropyl-1H-pyrrole-3-carbaldehyde

N-methylpyrrole aldehyde

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