1-Amino-4-(2-methylanilino)anthracene-9,10-dione

Base Information

Chemical Name:1-Amino-4-(2-methylanilino)anthracene-9,10-dione
CAS No.:54946-78-0
Molecular Formula:C₂₁H₁₆N₂O₂
Molecular Weight:328.37
Hs Code.:
DSSTox Substance ID:DTXSID30523737
Nikkaji Number:J33.346H
Wikidata:Q82390044

Synonyms:54946-78-0;1-Amino-4-(o-tolylamino)anthracene-9,10-dione;1-Amino-4-(2-methylanilino)anthracene-9,10-dione;DTXSID30523737

Suppliers and Price of 1-Amino-4-(2-methylanilino)anthracene-9,10-dione

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-Amino-4-(2-methylanilino)anthracene-9,10-dione

Chemical Property:

XLogP3:5.2
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:2
Exact Mass:328.121177757
Heavy Atom Count:25
Complexity:534

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1=CC=CC=C1NC2=C3C(=C(C=C2)N)C(=O)C4=CC=CC=C4C3=O

Technology Process of 1-Amino-4-(2-methylanilino)anthracene-9,10-dione

There total 3 articles about 1-Amino-4-(2-methylanilino)anthracene-9,10-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 95-53-4
o-toluidine

: 2872-47-1
1-amino-4-chloroanthraquinone

: 54946-78-0
1-amino-4-(o-toluidino)anthraquinone

Guidance literature:: With aluminium trichloride; Ambient temperature;

Reference yield:

: 2872-47-1
1-amino-4-chloroanthraquinone

: 54946-78-0
1-amino-4-(o-toluidino)anthraquinone

Guidance literature:: Multi-step reaction with 3 steps

1: 1) amyl nitrite 2) NaN₃ / 1)acetic acid, room temperature 2) 30 min

2: toluene / 2 h / Heating

3: 89 percent / dimethylformamide / 2 h / Heating

With sodium azide; n-Amyl nitrite; In N,N-dimethyl-formamide; toluene;
DOI:10.1007/BF00557740

Reference yield:

: 74386-36-0
1-azido-4-chloro-anthraquinone

: 54946-78-0
1-amino-4-(o-toluidino)anthraquinone

Guidance literature:: Multi-step reaction with 2 steps

1: toluene / 2 h / Heating

2: 89 percent / dimethylformamide / 2 h / Heating

In N,N-dimethyl-formamide; toluene;
DOI:10.1007/BF00557740