(E)-2,7-Octadienoic acid ethyl ester

Base Information

• Chemical Name: (E)-2,7-Octadienoic acid ethyl ester
• CAS No.: 55282-91-2
• Molecular Formula: C10H16O2
• Molecular Weight: 168.236
• Hs Code.: 2916190090
• Mol file: 55282-91-2.mol

Synonyms:5-hexen-1-ol;ethyl (2E)-2,7-octadienoate;ethyl (E)-2,7-octadienoate;2,7-Octadienoic acid,ethyl ester,(E);

Chemical Property of (E)-2,7-Octadienoic acid ethyl ester

Chemical Property:

• PSA: 26.30000
• LogP: 2.46200

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (E)-2,7-Octadienoic acid ethyl ester

There total 10 articles about (E)-2,7-Octadienoic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

5-Hexen-1-ol (821-41-0) + diethoxyphosphoryl-acetic acid ethyl ester (867-13-0) → ethyl (2E)-2,7-octadienoate (55282-91-2)

Guidance literature:

5-Hexen-1-ol; With oxalyl dichloride; dimethyl sulfoxide; triethylamine; In dichloromethane; at -78 - 20 ℃; Inert atmosphere;

diethoxyphosphoryl-acetic acid ethyl ester; With 1,8-diazabicyclo[5.4.0]undec-7-ene; lithium chloride; In acetonitrile; at 20 ℃; Inert atmosphere;

DOI:10.1039/c0ob00619j

Reference yield: 80.0%

5-Hexen-1-ol (821-41-0) + ethyl (triphenylphosphoranylidene)acetate (1099-45-2) → ethyl (2E)-2,7-octadienoate (55282-91-2)

Guidance literature:

With pyridine-SO₃ complex; triethylamine; In dichloromethane; dimethyl sulfoxide; at 20 ℃; for 3h;

DOI:10.1021/jo051566e

Reference yield:

diethoxyphosphoryl-acetic acid ethyl ester (867-13-0) + hex-5-en-1-al (764-59-0) → ethyl (2E)-2,7-octadienoate (55282-91-2)

Guidance literature:

With 1,8-diazabicyclo[5.4.0]undec-7-ene; lithium chloride; In acetonitrile; at 20 ℃;

DOI:10.1021/ol702299c

upstream raw materials:

hex-5-en-1-al

ethyl (triphenylphosphoranylidene)acetate

5-Hexen-1-ol

5-hydroxypentanal

Downstream raw materials:

(1S,2S,3S,4S)-4-aminocyclohexane-1,2,3-triol

(1S,2S,3S)-1-(2',2',2'-trichloromethylcarbonylamino)-2,3-dihydroxycyclohexane

(1S,2S,3S)-1-(2',2',2'-trichloromethylcarbonylamino)-2-hydroxy-3-iodocyclohexane

(1S,2R)-1-(2',2',2'-trichloromethylcarbonylamino)-2-hydroxycyclohex-3-ene

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