Hydroxylamine, O-[(3-fluorophenyl)methyl]-

Base Information

Chemical Name:Hydroxylamine, O-[(3-fluorophenyl)methyl]-
CAS No.:55418-29-6
Molecular Formula:C7H8FNO
Molecular Weight:141.145
Hs Code.:2922199090

Synonyms:O-(3-fluorobenzyl)-hydroxylamine;Chlorprazophos [ISO];Phosphorothioic acid,O-(3-chloro-7-methylpyrazolo(1,5-a)pyrimidin-2-yl) O,O-diethyl ester;thiophosphoric acid O-(3-chloro-7-methyl-pyrazolo[1,5-a]pyrimidin-2-yl) ester O',O''-diethyl ester;(3-chloro-6-methylpyrazolo[1,5-a]pyrimidin-2-yl)oxy-diethoxy-sulfanylidene;Chlorprazophos;O-(3-Chloro-7-methylpyrazolo(1,5-a)pyrimidin-2-yl) O,O-diethyl thiophosphate;3-fluorobenzyloxyamine;

Suppliers and Price of Hydroxylamine, O-[(3-fluorophenyl)methyl]-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
O-(3-FLUORO-BENZYL)-HYDROXYLAMINE 95.00%
5MG
$ 502.88

Total 0 raw suppliers

Chemical Property of Hydroxylamine, O-[(3-fluorophenyl)methyl]-

Chemical Property:

PSA：36.87000
LogP:-2.49680

Purity/Quality:: O-(3-FLUORO-BENZYL)-HYDROXYLAMINE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Hydroxylamine, O-[(3-fluorophenyl)methyl]-

There total 3 articles about Hydroxylamine, O-[(3-fluorophenyl)methyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 30777-87-8
2-(3-fluorobenzyloxy)isoindole-1,3-dione

: 55418-29-6
O-(3-fluorobenzyl)-hydroxylamine

Guidance literature:: With hydrazine hydrate; In ethanol; at 78 ℃;
DOI:10.1016/S0960-894X(03)00713-3

Reference yield: 42.0%

: 55418-29-6
O-(3-fluorobenzyl)-hydroxylamine

Guidance literature:: With N-hydroxyphthalimide; triphenylphosphine; diethylazodicarboxylate; In dichloromethane; at 20 ℃;

Reference yield:

: 456-47-3
3-fluoro-benzenemethanol

: 55418-29-6
O-(3-fluorobenzyl)-hydroxylamine

Guidance literature:: Multi-step reaction with 2 steps

1: PPh₃; DEAD / tetrahydrofuran / 0 - 50 °C

2: 80 percent / N₂H₄*H₂O / ethanol / 78 °C

With hydrazine hydrate; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; ethanol; 1: Mitsunobu reaction;
DOI:10.1016/S0960-894X(03)00713-3