4-(CHLOROMETHYL)-3-(4-CHLOROPHENYL)-1-PHENYL-1H-PYRAZOLE

Base Information

Chemical Name:4-(CHLOROMETHYL)-3-(4-CHLOROPHENYL)-1-PHENYL-1H-PYRAZOLE
CAS No.:55432-06-9
Molecular Formula:C16H12Cl2N2
Molecular Weight:303.191
Hs Code.:
Mol file:55432-06-9.mol

Synonyms:4-(CHLOROMETHYL)-3-(4-CHLOROPHENYL)-1-PHENYL-1H-PYRAZOLE;4-chloromethyl-3-(p-chlorophenyl)-1-phenylpyrazole;

Suppliers and Price of 4-(CHLOROMETHYL)-3-(4-CHLOROPHENYL)-1-PHENYL-1H-PYRAZOLE

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

AK Scientific
4-(Chloromethyl)-3-(4-chlorophenyl)-1-phenyl-1H-pyrazole
10g
$ 1045.00

Total 4 raw suppliers

Chemical Property of 4-(CHLOROMETHYL)-3-(4-CHLOROPHENYL)-1-PHENYL-1H-PYRAZOLE

Chemical Property:

PSA：17.82000
LogP:4.93150

Purity/Quality:

99% ^*data from raw suppliers

4-(Chloromethyl)-3-(4-chlorophenyl)-1-phenyl-1H-pyrazole ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 4-(CHLOROMETHYL)-3-(4-CHLOROPHENYL)-1-PHENYL-1H-PYRAZOLE

There total 6 articles about 4-(CHLOROMETHYL)-3-(4-CHLOROPHENYL)-1-PHENYL-1H-PYRAZOLE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 36640-39-8
4-hydroxy-methyl-1-phenyl-3-(p-chlorophenyl)-pyrazol

: 55432-06-9
4-(chloromethyl)-3-(4-chlorophenyl)-1-phenyl-1H-pyrazole

Guidance literature:: With thionyl chloride; In benzene; for 2.5h; Heating;

Reference yield:

: 36663-00-0
1-phenyl-3-(4-chlorophenyl)-4-pyrazolecarboxaldehyde

: 55432-06-9
4-(chloromethyl)-3-(4-chlorophenyl)-1-phenyl-1H-pyrazole

Guidance literature:: Multi-step reaction with 2 steps

1: 84 percent / sodium tetrahydridoborate / ethanol / 1 h

2: 79 percent / thionyl chloride / benzene / 2 h / Heating

With sodium tetrahydroborate; thionyl chloride; In ethanol; benzene;
DOI:10.1023/A:1016346528487

Reference yield:

: (E)-1-(1-(4-chlorophenyl)ethylidene)-2-phenylhydrazine

: 55432-06-9
4-(chloromethyl)-3-(4-chlorophenyl)-1-phenyl-1H-pyrazole

Guidance literature:: Multi-step reaction with 3 steps

1: POCl₃ / 1.) 30 min, room temp.; 2.) 2 h, 75 deg C

2: 99 percent / 97percent NaBH₄ / aq. ethanol / 0.5 h / 35 - 40 °C

3: 100 percent / SOCl₂ / benzene / 2.5 h / Heating

With sodium tetrahydroborate; thionyl chloride; trichlorophosphate; In ethanol; benzene;