4-[(4-nitrophenyl)amino]benzoic acid

Base Information

Chemical Name:4-[(4-nitrophenyl)amino]benzoic acid
CAS No.:16124-69-9
Molecular Formula:C13H10 N2 O4
Molecular Weight:258.233
Hs Code.:
Mol file:16124-69-9.mol

Synonyms:Benzoicacid, p-(p-nitroanilino)- (6CI,7CI,8CI); 4-Nitro-4'-diphenylaminecarboxylicacid; 4-[(4-Nitrophenyl)amino]benzoic acid; NSC 229460

Suppliers and Price of 4-[(4-nitrophenyl)amino]benzoic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of 4-[(4-nitrophenyl)amino]benzoic acid

Chemical Property:

Vapor Pressure:2.19E-10mmHg at 25°C
Boiling Point:489.2°Cat760mmHg
Flash Point:249.7°C
Density:1.435g/cm³

Purity/Quality:: 98%min ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 4-[(4-nitrophenyl)amino]benzoic acid

There total 6 articles about 4-[(4-nitrophenyl)amino]benzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 4-[(4-nitrophenyl)amino]benzoic acid methyl ester

: 16124-69-9
4-[(4-nitrophenyl)amino]benzoic acid

Guidance literature:: 4-[(4-nitrophenyl)amino]benzoic acid methyl ester; With potassium hydroxide; In ethanol; water; at 20 - 100 ℃; Inert atmosphere;

With hydrogenchloride; In water; at 0 ℃; pH=2; Inert atmosphere;
DOI:10.1021/jm201547v

Reference yield:

: 150-13-0,159246-81-8,8014-65-1
4-amino-benzoic acid

: 350-46-9,178603-76-4
4-Fluoronitrobenzene

: 16124-69-9
4-[(4-nitrophenyl)amino]benzoic acid

Guidance literature:: With magnesium oxide; sodium carbonate;

Reference yield:

: 619-42-1
4-methoxycarbonylphenyl bromide

: 100-01-6,104810-17-5
4-nitro-aniline

: 16124-69-9
4-[(4-nitrophenyl)amino]benzoic acid

Guidance literature:: Multi-step reaction with 2 steps

1.1: palladium diacetate; caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl / toluene / 20 - 120 °C / Inert atmosphere

2.1: potassium hydroxide / ethanol; water / 20 - 100 °C / Inert atmosphere

2.2: 0 °C / pH 2 / Inert atmosphere

With palladium diacetate; caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; potassium hydroxide; In ethanol; water; toluene; 1.1: Buchwald-Hartwig reaction;
DOI:10.1021/jm201547v