Benzonitrile, 3-(phenylazo)-

Base Information

Chemical Name:Benzonitrile, 3-(phenylazo)-
CAS No.:55669-57-3
Molecular Formula:C13H9N3
Molecular Weight:207.235
Hs Code.:
DSSTox Substance ID:DTXSID50464370
Nikkaji Number:J1.696.008J

Synonyms:Benzonitrile, 3-(phenylazo)-;55669-57-3;3-phenyldiazenylbenzonitrile;DTXSID50464370

Suppliers and Price of Benzonitrile, 3-(phenylazo)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of Benzonitrile, 3-(phenylazo)-

Chemical Property:

XLogP3:3.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:2
Exact Mass:207.079647300
Heavy Atom Count:16
Complexity:283

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=CC=C(C=C1)N=NC2=CC=CC(=C2)C#N

Technology Process of Benzonitrile, 3-(phenylazo)-

There total 5 articles about Benzonitrile, 3-(phenylazo)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: C₆H₅NN(C(CH₃)3CO₂)2C₆H₄CN

: 55669-57-3
3-Cyanoazobenzol

Guidance literature:: With copper(l) iodide; caesium carbonate; In N,N-dimethyl-formamide; at 110 ℃; for 24h;
DOI:10.1016/j.tetlet.2003.10.091

Reference yield: 60.0%

: 65578-58-7
di-tert-butyl 1-phenylhydrazine-1,2-dicarboxylate

: 69113-59-3
3-iodobenzonitrile

: 55669-57-3
3-Cyanoazobenzol

Guidance literature:: With copper(l) iodide; 1,10-Phenanthroline; caesium carbonate; In N,N-dimethyl-formamide; at 110 ℃; for 72h;
DOI:10.1016/j.tetlet.2003.10.091

Reference yield:

: 65578-58-7
di-tert-butyl 1-phenylhydrazine-1,2-dicarboxylate

: 55669-57-3
3-Cyanoazobenzol

Guidance literature:: Multi-step reaction with 2 steps

1: 99 percent / 1,10-phenanthroline; Cs₂CO₃; CuI / dimethylformamide / 3 h / 80 °C

2: 63 percent / CuI; Cs₂CO₃ / dimethylformamide / 24 h / 110 °C

With copper(l) iodide; 1,10-Phenanthroline; caesium carbonate; In N,N-dimethyl-formamide;
DOI:10.1016/j.tetlet.2003.10.091