2-Anilino-6-chloro-3-nitrobenzoic acid

Base Information

Chemical Name:2-Anilino-6-chloro-3-nitrobenzoic acid
CAS No.:55776-07-3
Molecular Formula:C13H9ClN2O4
Molecular Weight:292.678
Hs Code.:
DSSTox Substance ID:DTXSID30538907
Wikidata:Q82414480

Synonyms:55776-07-3;2-Anilino-6-chloro-3-nitrobenzoic acid;DTXSID30538907;6-CHLORO-3-NITRO-2-(PHENYLAMINO)BENZOIC ACID

Suppliers and Price of 2-Anilino-6-chloro-3-nitrobenzoic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 2-Anilino-6-chloro-3-nitrobenzoic acid

Chemical Property:

Melting Point:206 °C
Boiling Point:428.4±45.0 °C(Predicted)
PSA：95.15000
Density:1.525±0.06 g/cm3(Predicted)
LogP:4.28620
XLogP3:4
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:3
Exact Mass:292.0250845
Heavy Atom Count:20
Complexity:368

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)NC2=C(C=CC(=C2C(=O)O)Cl)[N+](=O)[O-]

Technology Process of 2-Anilino-6-chloro-3-nitrobenzoic acid

There total 4 articles about 2-Anilino-6-chloro-3-nitrobenzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 55775-97-8
2,6-dichloro-3-nitrobenzoic acid

: 62-53-3
aniline

: 55776-07-3
6-chloro-3-nitro-2-(phenylamino)benzoic acid

Guidance literature:: at 125 - 130 ℃; for 0.333333h;

Reference yield:

: 20443-98-5
2,6-Dichlorobenzyl bromide

: 55776-07-3
6-chloro-3-nitro-2-(phenylamino)benzoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: potassium acetate; ethanol / Erwaermen des Reaktionsprodukts mit wss. Natronlauge und Behandeln des Reaktionsgemisches mit Kaliumpermanganat

2: concentrated sulfuric acid; nitric acid

3: 135 °C

With ethanol; sulfuric acid; nitric acid; potassium acetate;
DOI:10.1007/BF02809653

Reference yield:

: 50-30-6
2,6-dichlorobenzoic acid

: 55776-07-3
6-chloro-3-nitro-2-(phenylamino)benzoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: concentrated sulfuric acid; nitric acid

2: 135 °C

With sulfuric acid; nitric acid;
DOI:10.1007/BF02809653