Ethanone, 1-(1-cyclohepten-1-yl)-2-phenyl-

Base Information

Chemical Name:Ethanone, 1-(1-cyclohepten-1-yl)-2-phenyl-
CAS No.:55980-52-4
Molecular Formula:C15H18O
Molecular Weight:214.307
Hs Code.:

Synonyms:

Suppliers and Price of Ethanone, 1-(1-cyclohepten-1-yl)-2-phenyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Ethanone, 1-(1-cyclohepten-1-yl)-2-phenyl-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Ethanone, 1-(1-cyclohepten-1-yl)-2-phenyl-

There total 4 articles about Ethanone, 1-(1-cyclohepten-1-yl)-2-phenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 72946-37-3
1-hydroxy-1-(2-phenylethynyl)cycloheptane

: 55980-52-4
1-(1-oxo-2-phenylethyl)cyclohept-1-ene

Guidance literature:: With 1-methyl-3-(4-sulfonylbutyl)-1H-imidazol-3-ium trifluoromethanesulfonate; 3-butyl-1-methyl-1H-imidazol-3-ium hexafluorophosphate; at 20 - 75 ℃; for 5h; Schlenk technique;
DOI:10.1016/j.tetlet.2013.09.028

Reference yield:

: 502-42-1
cycloheptanone

: 55980-52-4
1-(1-oxo-2-phenylethyl)cyclohept-1-ene

Guidance literature:: Multi-step reaction with 2 steps

1: 45 percent / n-butyllithium / tetrahydrofuran; hexane / 0 deg C, 75 min then rt., 3.5 h

2: 40 percent / 90percent aq. formic acid / 3 h / Heating

With n-butyllithium; formic acid; In tetrahydrofuran; hexane;
DOI:10.1016/S0040-4020(01)80560-3

Reference yield:

: 502-42-1
cycloheptanone

: 55980-52-4
1-(1-oxo-2-phenylethyl)cyclohept-1-ene

Guidance literature:: Multi-step reaction with 2 steps

1.1: tetrabutyl ammonium fluoride; potassium hydroxide / tetrahydrofuran / 12 h / 20 °C / Inert atmosphere

1.2: 72 h / 20 °C / Inert atmosphere

2.1: 3-butyl-1-methyl-1H-imidazol-3-ium hexafluorophosphate; 1-methyl-3-(4-sulfonylbutyl)-1H-imidazol-3-ium trifluoromethanesulfonate / 5 h / 20 - 75 °C / Schlenk technique

With 1-methyl-3-(4-sulfonylbutyl)-1H-imidazol-3-ium trifluoromethanesulfonate; tetrabutyl ammonium fluoride; 3-butyl-1-methyl-1H-imidazol-3-ium hexafluorophosphate; potassium hydroxide; In tetrahydrofuran; 2.1: |Rupe Rearrangement;
DOI:10.1016/j.tetlet.2013.09.028