1,2-Cyclotridecadiene

Base Information

Chemical Name:1,2-Cyclotridecadiene
CAS No.:5601-67-2
Molecular Formula:C13H22
Molecular Weight:178.318
Hs Code.:
DSSTox Substance ID:DTXSID40446009
Nikkaji Number:J81.061D,J82.762B
Mol file:5601-67-2.mol

Synonyms:1,2-cyclotridecadiene;Cyclotrideca-1,2-diene;[R,(+)]-1,2-Cyclotridecadiene;5601-67-2;18526-51-7;DTXSID40446009

Suppliers and Price of 1,2-Cyclotridecadiene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 1,2-Cyclotridecadiene

Chemical Property:

PSA：0.00000
LogP:4.61230
XLogP3:5.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:0
Exact Mass:178.172150702
Heavy Atom Count:13
Complexity:139

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1CCCCCC=C=CCCCC1

Technology Process of 1,2-Cyclotridecadiene

There total 8 articles about 1,2-Cyclotridecadiene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 17301-57-4
13,13-dibromobicyclo<10.1.0>tridecane

: 5601-67-2
cyclotrideca-1,2-diene

Guidance literature:: With methyllithium; In diethyl ether; at -78 - 20 ℃; for 1.33333h;
DOI:10.1002/anie.201812984 DOI:10.1002/anie.201903365

Reference yield:

: 17301-57-4
13,13-dibromobicyclo<10.1.0>tridecane

: 3105-35-9
bicyclo<10.1.0>tridecane

: 5601-67-2
cyclotrideca-1,2-diene

: 54766-91-5
bicyclo[10.1.0]tridec-1-ene

Guidance literature:: With zinc; In N,N-dimethyl-formamide; at 130 ℃; for 4h;

Reference yield:

: 1501-82-2
cyclododecene

: 5601-67-2
cyclotrideca-1,2-diene

Guidance literature:: Multi-step reaction with 2 steps

1: N-benzyl-N,N,N-triethylammonium chloride; potassium hydroxide / ethanol; water / 16 h / 0 - 20 °C

2: methyllithium / diethyl ether / 1.33 h / -78 - 20 °C

With N-benzyl-N,N,N-triethylammonium chloride; methyllithium; potassium hydroxide; In diethyl ether; ethanol; water;
DOI:10.1002/anie.201812984