Cyclotridecyne

Base Information

Chemical Name:Cyclotridecyne
CAS No.:5601-68-3
Molecular Formula:C13H22
Molecular Weight:178.318
Hs Code.:
DSSTox Substance ID:DTXSID80455751
Nikkaji Number:J811.044A
Wikidata:Q82277874

Synonyms:Cyclotridecyne;Cyclotridec-1-yne;5601-68-3;DTXSID80455751

Suppliers and Price of Cyclotridecyne

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Cyclotridecyne

Chemical Property:

XLogP3:5.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:0
Exact Mass:178.172150702
Heavy Atom Count:13
Complexity:151

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1CCCCCC#CCCCCC1

Technology Process of Cyclotridecyne

There total 1 articles about Cyclotridecyne which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 33.0%

: 830-13-7
cyclododecanone

: 18107-18-1
diazomethyl-trimethyl-silane

: 5601-68-3
cyclotridecyne

: 5037-22-9
formyl cyclododecane

: 1266615-06-8
(2-cyclododecylidenevinyl)trimethylsilane

: bicyclo[8.2.1]tridec-1⁽¹³⁾-ene

Guidance literature:: diazomethyl-trimethyl-silane; With lithium diisopropyl amide; In hexane; N,N-dimethyl-formamide; at -78 ℃; for 0.5h;

cyclododecanone; In tetrahydrofuran; hexane; N,N-dimethyl-formamide; at -78 ℃; for 4h; Reflux;
DOI:10.1021/acs.joc.7b00346

Reference yield: 49.0%

: 5601-68-3
cyclotridecyne

: 165554-70-1
6-ethoxy-3-phenyl-6H-1,2-oxazine

: 1352703-59-3
2-phenyl-6,7,8,9,10,11,12,13,14,15-decahydro-5H-1-azabenzocyclotridecene

Guidance literature:: With boron trifluoride diethyl etherate; In 1,2-dichloro-ethane; at 70 ℃; for 1h; Microwave irradiation; Inert atmosphere;
DOI:10.1002/ejoc.201100765