1,3,2-Benzodioxaborole, 2-hexyl-

Base Information

Chemical Name:1,3,2-Benzodioxaborole, 2-hexyl-
CAS No.:56554-22-4
Molecular Formula:C12H17BO2
Molecular Weight:204.077
Hs Code.:
DSSTox Substance ID:DTXSID40451714
Nikkaji Number:J1.173.640H
Wikidata:Q82271881

Synonyms:1,3,2-Benzodioxaborole, 2-hexyl-;56554-22-4;2-HEXYL-1,3,2-BENZODIOXABOROLE;DTXSID40451714

Suppliers and Price of 1,3,2-Benzodioxaborole, 2-hexyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of 1,3,2-Benzodioxaborole, 2-hexyl-

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:5
Exact Mass:204.1321599
Heavy Atom Count:15
Complexity:173

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:B1(OC2=CC=CC=C2O1)CCCCCC

Technology Process of 1,3,2-Benzodioxaborole, 2-hexyl-

There total 1 articles about 1,3,2-Benzodioxaborole, 2-hexyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 592-41-6,25067-06-5
1-hexene

: 274-07-7
benzo[1,3,2]dioxaborole

: 592-47-2
3-hexene

: 56554-22-4
B-n-hexylcatecholborane

: 592-43-8
2-hexene

Guidance literature:: With C₂₁H₄₆MoNP₃; In benzene-d6; at 22 ℃; for 24h; Reagent/catalyst; Time; Catalytic behavior; Inert atmosphere;
DOI:10.1039/c5dt02945g

Reference yield:

: 56554-22-4
B-n-hexylcatecholborane

: 106-51-4
p-benzoquinone

: 4197-72-2
2-hexylhydroquinone

Guidance literature:: With 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; In tetrahydrofuran; at 20 ℃; for 2h; Schlenk technique;
DOI:10.1016/j.tet.2018.01.048

Reference yield:

: 56554-22-4
B-n-hexylcatecholborane

: [(3-chloro-1-methylenenonyl)sulfonyl]benzene

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 0.08 h / -100 °C / Inert atmosphere

1.2: -100 - 20 °C / Inert atmosphere

2.1: di-tert-butoxydiazene / N,N-dimethyl-formamide; chlorobenzene / 4 h / 60 °C / Inert atmosphere

With n-butyllithium; di-tert-butoxydiazene; In tetrahydrofuran; hexane; N,N-dimethyl-formamide; chlorobenzene;
DOI:10.1021/acs.joc.5b02610