2-Phenylcyclopropanecarbonyl chloride

Base Information

Chemical Name:2-Phenylcyclopropanecarbonyl chloride
CAS No.:5685-36-9
Molecular Formula:C₁₀H₉ClO
Molecular Weight:180.634
Hs Code.:
Mol file:5685-36-9.mol

Synonyms:Cyclopropanecarbonyl chloride,2-phenyl;2-phenylcyclopropanecarbonyl chloride;trans-2-phenylcyclopropanecarbonyl chloride;Cyclopropanecarbonyl chloride,2-phenyl-,trans;trans-2-phenylcyclopropanecarboxylic acid chloride;trans-2-phenyl-1-cyclopropanecarbonyl chloride;

Suppliers and Price of 2-Phenylcyclopropanecarbonyl chloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
2-Phenylcyclopropanecarbonylchloride
100mg
$ 310.00

Matrix Scientific
2-Phenylcyclopropanecarbonyl chloride 97%
1g
$ 575.00

Matrix Scientific
2-Phenylcyclopropanecarbonyl chloride 97%
500mg
$ 374.00

Atlantic Research Chemicals
2-Phenylcyclopropanecarbonylchloride 95%
1gm:
$ 258.02

Atlantic Research Chemicals
2-Phenylcyclopropanecarbonylchloride 95%
250mgs:
$ 134.31

Total 6 raw suppliers

Chemical Property of 2-Phenylcyclopropanecarbonyl chloride

Chemical Property:

PSA：17.07000
LogP:2.55550

Purity/Quality:

99%, ^*data from raw suppliers

2-Phenylcyclopropanecarbonylchloride ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2-Phenylcyclopropanecarbonyl chloride

There total 8 articles about 2-Phenylcyclopropanecarbonyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 939-90-2
trans-2-phenylcyclopropane-1-carboxylic acid

: 939-87-7,5685-36-9,37107-48-5,42916-08-5,42916-12-1,42916-13-2,62624-90-2,78738-39-3
(1SR,2SR)-2-phenylcyclopropanecarbonyl chloride

Guidance literature:: With thionyl chloride; In N,N-dimethyl-formamide; benzene; for 3h; Heating;
DOI:10.1021/ja00053a031

Reference yield:

: 140-10-3
(E)-3-phenylacrylic acid

: 939-87-7,5685-36-9,37107-48-5,42916-08-5,42916-12-1,42916-13-2,62624-90-2,78738-39-3
(1SR,2SR)-2-phenylcyclopropanecarbonyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1: CuCr₂O₄; 1-butyl-3-methylimidazolium hydroxide / tetrahydrofuran / 4 h / 20 - 50 °C

2: chloroformic acid ethyl ester; triethylamine / toluene / 4 h / Cooling with ice

With 1-butyl-3-methylimidazolium hydroxide; CuCr₂O₄; chloroformic acid ethyl ester; triethylamine; In tetrahydrofuran; toluene;
DOI:10.1007/s11164-016-2572-1