7-Methoxynaphthalene-1-sulfonyl chloride

Base Information

Chemical Name:7-Methoxynaphthalene-1-sulfonyl chloride
CAS No.:56875-61-7
Molecular Formula:C₁₁H₉ClO₃S
Molecular Weight:256.71
Hs Code.:
DSSTox Substance ID:DTXSID70593010
Nikkaji Number:J469.316G
Wikidata:Q82487384

Synonyms:7-Methoxynaphthalene-1-sulfonyl chloride;56875-61-7;SCHEMBL2328914;DTXSID70593010

Suppliers and Price of 7-Methoxynaphthalene-1-sulfonyl chloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of 7-Methoxynaphthalene-1-sulfonyl chloride

Chemical Property:

XLogP3:3.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:2
Exact Mass:255.9960930
Heavy Atom Count:16
Complexity:336

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:COC1=CC2=C(C=CC=C2S(=O)(=O)Cl)C=C1

Technology Process of 7-Methoxynaphthalene-1-sulfonyl chloride

There total 2 articles about 7-Methoxynaphthalene-1-sulfonyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: Sodium; 7-methoxy-naphthalene-1-sulfonate

: 56875-61-7
7-methoxy-naphthalene-1-sulfonyl chloride

Guidance literature:: With thionyl chloride; In N,N-dimethyl-formamide; for 3h; Ambient temperature;
DOI:10.1021/jo00035a018

Reference yield:

: 832-85-9
2-hydroxy-8-naphthalenesulfonic acid monosodium salt

: 56875-61-7
7-methoxy-naphthalene-1-sulfonyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1: NaOH / H₂O / 1 h / 50 - 55 °C

2: thionyl chloride / dimethylformamide / 3 h / Ambient temperature

With sodium hydroxide; thionyl chloride; In water; N,N-dimethyl-formamide;
DOI:10.1021/jo00035a018