2-(2-(broMoMethyl)phenyl)isoindoline-1,3-dione

Base Information

• Chemical Name: 2-(2-(broMoMethyl)phenyl)isoindoline-1,3-dione
• CAS No.: 57365-06-7
• Molecular Formula: C15H10BrNO2
• Molecular Weight: 316.154
• Hs Code.: 2925190090
• Mol file: 57365-06-7.mol

Synonyms:o-phthalimidobenzyl bromide;2-phthalimidobenzylbromide;o-N-phatalimidobenzyl bromide;

Chemical Property of 2-(2-(broMoMethyl)phenyl)isoindoline-1,3-dione

Chemical Property:

• PSA: 37.38000
• LogP: 3.44710

Purity/Quality:

97% ^*data from raw suppliers

2-(2-(Bromomethyl)phenyl)isoindoline-1,3-dione ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-(2-(broMoMethyl)phenyl)isoindoline-1,3-dione

There total 2 articles about 2-(2-(broMoMethyl)phenyl)isoindoline-1,3-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

N-(2-methylphenyl)phthalimide (2464-33-7) → 2-<2-(bromomethyl)phenyl>-1H-isoindole-1,3(2H)-dione (57365-06-7)

Guidance literature:

With N-Bromosuccinimide; dibenzoyl peroxide; In benzene; for 1.5h; Microwave irradiation; Reflux;

DOI:10.1080/00397911.2010.517378

Reference yield:

→ 2-<2-(bromomethyl)phenyl>-1H-isoindole-1,3(2H)-dione (57365-06-7)

Guidance literature:

N-o-Tolylphthalimid, NBS;

Reference yield: 95.0%

2-<2-(bromomethyl)phenyl>-1H-isoindole-1,3(2H)-dione (57365-06-7) + triethyl phosphite (122-52-1) → diethyl <<2-(1,3-dihydro-1,3-dioxo-2H-isoindol-2-yl)phenyl>methyl>phosphonate (140150-99-8)

Guidance literature:

at 100 ℃; for 3h;

DOI:10.1021/jm00086a005

upstream raw materials:

N-(2-methylphenyl)phthalimide

Downstream raw materials:

2-(2'-phthalimidobenzylamino)-benzyl alcohol

N-(2-methylphenyl)phthalimide

methyl (2-phthalimidobenzyl)phenylphosphinate

2-phthalimidobenzylidene bromide

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