Benzeneacetonitrile, 2-(2-naphthalenylthio)-

Base Information

Chemical Name:Benzeneacetonitrile, 2-(2-naphthalenylthio)-
CAS No.:57536-27-3
Molecular Formula:C18H13NS
Molecular Weight:275.374
Hs Code.:
DSSTox Substance ID:DTXSID20481397

Synonyms:57536-27-3;2-(2-(naphthalen-2-ylthio)phenyl)acetonitrile;2-[2-(NAPHTHALEN-2-YLSULFANYL)PHENYL]ACETONITRILE;Benzeneacetonitrile, 2-(2-naphthalenylthio)-;SCHEMBL5659555;DTXSID20481397

Suppliers and Price of Benzeneacetonitrile, 2-(2-naphthalenylthio)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of Benzeneacetonitrile, 2-(2-naphthalenylthio)-

Chemical Property:

XLogP3:4.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:275.07687059
Heavy Atom Count:20
Complexity:358

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C2C=C(C=CC2=C1)SC3=CC=CC=C3CC#N

Technology Process of Benzeneacetonitrile, 2-(2-naphthalenylthio)-

There total 7 articles about Benzeneacetonitrile, 2-(2-naphthalenylthio)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 773837-37-9
sodium cyanide

: 613670-87-4
2-(2-bromomethyl-phenylsulfanyl)-naphthalene

: 57536-27-3
[2-(naphthalene-2-ylsulfanyl) phenyl]-acetonitrile

Guidance literature:: In ethanol; for 4h; Reflux;
DOI:10.3987/COM-10-12014

Reference yield:

: 613670-87-4
2-(2-bromomethyl-phenylsulfanyl)-naphthalene

: 143-33-9,25596-52-5
sodium cyanide

: 57536-27-3
[2-(naphthalene-2-ylsulfanyl) phenyl]-acetonitrile

Guidance literature:: In ethanol; for 3h; Heating / reflux;

Reference yield:

: 88-67-5
2-Iodobenzoic acid

: 57536-27-3
[2-(naphthalene-2-ylsulfanyl) phenyl]-acetonitrile

Guidance literature:: Multi-step reaction with 4 steps

1: (i) aq. KOH, (ii) /BRN= 1861406/, Cu

2: LiAlH₄

3: SOCl₂

4: dimethylformamide

With lithium aluminium tetrahydride; thionyl chloride; In N,N-dimethyl-formamide;
DOI:10.1135/cccc19751960