(R)-(+)-1-(2-PYRROLIDINYLMETHYL)PIPERIDINE

Base Information

• Chemical Name: (R)-(+)-1-(2-PYRROLIDINYLMETHYL)PIPERIDINE
• CAS No.: 575469-26-0
• Molecular Formula: C10H20N2
• Molecular Weight: 168.27900
• Hs Code.: 2933399990
• Mol file: 575469-26-0.mol

Synonyms:SS-METHYLAZETIDIN-2-ONE;1-Bma Or 4-Bma;1-BMA;B-METHYLAZETIDIN-2-ONE;4-BMA;Side chain for iMipe;

Chemical Property of (R)-(+)-1-(2-PYRROLIDINYLMETHYL)PIPERIDINE

Chemical Property:

• PSA: 15.27000
• LogP: 1.49100

Purity/Quality:

99% ^*data from raw suppliers

(R)-1-[(Pyrrolidin-2-yl)methyl]piperidinedihydrochloride ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of (R)-(+)-1-(2-PYRROLIDINYLMETHYL)PIPERIDINE

There total 5 articles about (R)-(+)-1-(2-PYRROLIDINYLMETHYL)PIPERIDINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Fasoracetam (110958-19-5) → (R)-2-[(piperidin-1-yl)methyl]pyrrolidine (575469-26-0)

Guidance literature:

With lithium aluminium tetrahydride; In tetrahydrofuran; for 4h; Heating;

DOI:10.1016/S0957-4166(02)00579-7

Reference yield:

piperidine (110-89-4) → (R)-2-[(piperidin-1-yl)methyl]pyrrolidine (575469-26-0)

Guidance literature:

Multi-step reaction with 2 steps

1: acetonitrile / 0.17 h / 20 °C

2: LiAlH₄ / tetrahydrofuran / 4 h / Heating

With lithium aluminium tetrahydride; In tetrahydrofuran; acetonitrile;

DOI:10.1016/S0957-4166(02)00579-7

Reference yield:

D-pyrrolidone-5-carboxylic acid (4042-36-8) → (R)-2-[(piperidin-1-yl)methyl]pyrrolidine (575469-26-0)

Guidance literature:

Multi-step reaction with 3 steps

1: PTSA / toluene / 16 h / Heating

2: acetonitrile / 0.17 h / 20 °C

3: LiAlH₄ / tetrahydrofuran / 4 h / Heating

With lithium aluminium tetrahydride; toluene-4-sulfonic acid; In tetrahydrofuran; toluene; acetonitrile;

DOI:10.1016/S0957-4166(02)00579-7

upstream raw materials:

Fasoracetam

piperidine

D-pyrrolidone-5-carboxylic acid

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