1,3-Bis(2-methoxyphenoxy)propan-2-one

Base Information

Chemical Name:1,3-Bis(2-methoxyphenoxy)propan-2-one
CAS No.:57641-30-2
Molecular Formula:C17H18O5
Molecular Weight:302.327
Hs Code.:
ChEMBL ID:CHEMBL3249579
DSSTox Substance ID:DTXSID60544814
Nikkaji Number:J453.011J
Wikidata:Q82422091

Synonyms:1,3-Bis(2-methoxyphenoxy)propan-2-one;57641-30-2;CHEMBL3249579;SCHEMBL10509566;DTXSID60544814

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,3-Bis(2-methoxyphenoxy)propan-2-one

Chemical Property:

XLogP3:3.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:8
Exact Mass:302.11542367
Heavy Atom Count:22
Complexity:303

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=CC=CC=C1OCC(=O)COC2=CC=CC=C2OC

Technology Process of 1,3-Bis(2-methoxyphenoxy)propan-2-one

There total 2 articles about 1,3-Bis(2-methoxyphenoxy)propan-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 16929-60-5
1,3-bis(o-methoxyphenoxy)-2-propanol

: 57641-30-2
1,3-bis(o-methoxyphenoxy)-2-propanone

Guidance literature:: With sodium acetate; magnesium sulfate; pyridinium chlorochromate; In dichloromethane; for 48h; Ambient temperature;
DOI:10.1021/ac00031a021

Reference yield:

: 90-05-1
2-methoxy-phenol

: 57641-30-2
1,3-bis(o-methoxyphenoxy)-2-propanone

Guidance literature:: Multi-step reaction with 2 steps

1: (i) NaOH, dioxane, (ii) /BRN= 79785/

2: DCC, DMSO, CF₃CO₂H / pyridine; diethyl ether

With dimethyl sulfoxide; dicyclohexyl-carbodiimide; trifluoroacetic acid; In pyridine; diethyl ether;
DOI:10.1021/jm00224a006

Reference yield:

: 57641-30-2
1,3-bis(o-methoxyphenoxy)-2-propanone

: 139376-35-5
4,4-bis<(o-methoxyphenoxy)methyl>-3-oxaheptanoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) magnesium / 1.) THF, reflux, 2.) THF, reflux, 5 h

2: 1.) KH / 1.) THF, 2 h, room temperature, 2.) THF, 3 h

With potassium hydride; magnesium;
DOI:10.1021/ac00031a021