Technology Process of 4-Bromobenzene-1-selenenyl chloride
There total 5 articles about 4-Bromobenzene-1-selenenyl chloride which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sulfuryl dichloride;
In
tetrachloromethane;
for 0.5h;
Ambient temperature;
DOI:10.1021/jo00171a002
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1) Mg, 2) Se / 1) Et2O, 2) Et2O, 20 min
2: NaOH, 3percent H2O2 / H2O / Ambient temperature; overnight
3: SO2Cl2 / CCl4 / 0.5 h / Ambient temperature
With
sodium hydroxide; selenium; sulfuryl dichloride; dihydrogen peroxide; magnesium;
In
tetrachloromethane; water;
DOI:10.1021/jo00171a002
- Guidance literature:
-
Multi-step reaction with 2 steps
1: NaOH, 3percent H2O2 / H2O / Ambient temperature; overnight
2: SO2Cl2 / CCl4 / 0.5 h / Ambient temperature
With
sodium hydroxide; sulfuryl dichloride; dihydrogen peroxide;
In
tetrachloromethane; water;
DOI:10.1021/jo00171a002
