2-NITROBENZENESULFONYL HYDRAZINE

Base Information

• Chemical Name: 2-NITROBENZENESULFONYL HYDRAZINE
• CAS No.: 6655-77-2
• Molecular Formula: C6H7N3O4S
• Molecular Weight: 217.205
• Hs Code.: 2935009090
• Mol file: 6655-77-2.mol

Synonyms:Benzenesulfonicacid, m-nitro-, hydrazide (7CI,8CI);3-Nitrobenzenesulfonic acid hydrazide;3-Nitrobenzenesulfonyl hydrazide;NSC 268248;m-Nitrobenzenesulfonic acidhydrazide;m-Nitrobenzenesulfonyl hydrazide;

Chemical Property of 2-NITROBENZENESULFONYL HYDRAZINE

Chemical Property:

• Vapor Pressure: 2.54E-07mmHg at 25°C
• Refractive Index: 1.62
• Boiling Point: 421.8 °C at 760 mmHg
• Flash Point: 208.9 °C
• PSA: 126.39000
• Density: 1.562 g/cm³
• LogP: 2.44200
• Storage Temp.: Keep in dark place,Inert atmosphere,Room temperature

Purity/Quality:

97% ^*data from raw suppliers

3-Nitrobenzenesulfonohydrazide ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-NITROBENZENESULFONYL HYDRAZINE

There total 2 articles about 2-NITROBENZENESULFONYL HYDRAZINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

3-nitrobenzenesulphonyl chloride (121-51-7) → 3-nitrophenylsulfonohydrazide (6655-77-2)

Guidance literature:

With hydrazine hydrate; In tetrahydrofuran; at 0 ℃;

DOI:10.1016/j.electacta.2020.137582

Reference yield:

→ 3-nitrophenylsulfonohydrazide (6655-77-2)

Guidance literature:

aus 3-Nitro-benzolsulfonylchlorid u. Hydrazinhydrat in Me.;

Reference yield: 98.0%

3-nitrophenylsulfonohydrazide (6655-77-2) → 3-nitrobenzenesulphonyl chloride (121-51-7)

Guidance literature:

With N-chloro-succinimide; In acetonitrile; at 20 ℃; for 2h;

DOI:10.3390/molecules26185551

upstream raw materials:

3-nitrobenzenesulphonyl chloride

Downstream raw materials:

piperonal-(3-nitro-benzenesulfonylhydrazone)

bis(3-nitrophenyl) disulfide

3-nitro-benzenethiosulfonic acid S-(3-nitro-phenyl ester)

N-acetyl-N'-(3-nitro-benzenesulfonyl)-hydrazine