3-Phenyl-2-[(trimethylsilyl)oxy]-1,3,2-oxazaphospholidine

Base Information

• Chemical Name: 3-Phenyl-2-[(trimethylsilyl)oxy]-1,3,2-oxazaphospholidine
• CAS No.: 58068-64-7
• Molecular Formula: C11H18NO2PSi
• Molecular Weight: 255.329
• DSSTox Substance ID: DTXSID00500111

Synonyms:58068-64-7;DTXSID00500111;3-Phenyl-2-[(trimethylsilyl)oxy]-1,3,2-oxazaphospholidine

Chemical Property of 3-Phenyl-2-[(trimethylsilyl)oxy]-1,3,2-oxazaphospholidine

Chemical Property:

• PSA: 35.29000
• LogP: 3.66660
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 3
• Exact Mass: 255.08444235
• Heavy Atom Count: 16
• Complexity: 229

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: C[Si](C)(C)OP1N(CCO1)C2=CC=CC=C2

Technology Process of 3-Phenyl-2-[(trimethylsilyl)oxy]-1,3,2-oxazaphospholidine

There total 3 articles about 3-Phenyl-2-[(trimethylsilyl)oxy]-1,3,2-oxazaphospholidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-chloro-3-phenyl-[1,3,2]oxazaphospholidine (31707-07-0) + N,N-bis(trimethylsilyl)acetamide (10416-58-7) → 2-trimethylsiloxy-3-phenyl-1,3,2-oxazaphospholane (58068-64-7)

Guidance literature:

Heating;

DOI:10.1007/BF01179480

Reference yield:

N,N-diethyl-1,1,1-trimethylsilanamine (996-50-9) + 2-oxo-2-hydro-3-phenyl-1,3,2-oxazaphospholane (51104-85-9) → 2-trimethylsiloxy-3-phenyl-1,3,2-oxazaphospholane (58068-64-7)

Guidance literature:

Reference yield:

→ 2-trimethylsiloxy-3-phenyl-1,3,2-oxazaphospholane (58068-64-7)

Guidance literature:

2-Chlor-3-phenyl-1,3,2-oxazaphospholan, N,N-Di-acetamid, 1Stg Δ 100-110grad;

upstream raw materials:

2-chloro-3-phenyl-[1,3,2]oxazaphospholidine

N,N-bis(trimethylsilyl)acetamide

N,N-diethyl-1,1,1-trimethylsilanamine

2-oxo-2-hydro-3-phenyl-1,3,2-oxazaphospholane

Downstream raw materials:

3-phenyl-2-(phenyl-trimethylsilanyloxy-methyl)-[1,3,2]oxazaphospholidine 2-oxide

phenyltrimethylsilyl ether

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