4-(bromomethyl)-1-(2,3,4,6-tetra-O-acetylhexopyranosyl)-1H-1,2,3-triazole

Base Information

• Chemical Name: 4-(bromomethyl)-1-(2,3,4,6-tetra-O-acetylhexopyranosyl)-1H-1,2,3-triazole
• CAS No.: 70380-26-6
• Molecular Formula: C₁₇H₂₂BrN₃O₉
• Molecular Weight: 492.28

Synonyms:1H-1,2,3-Triazole, 4-(bromomethyl)-1-(2,3,4, 6-tetra-O-acetyl-.beta.-D-glucopyranosyl)-;

Chemical Property of 4-(bromomethyl)-1-(2,3,4,6-tetra-O-acetylhexopyranosyl)-1H-1,2,3-triazole

Chemical Property:

• Vapor Pressure: 2.28E-12mmHg at 25°C
• Refractive Index: 1.602
• Boiling Point: 555.2°Cat760mmHg
• Flash Point: 289.6°C
• Density: 1.64g/cm³

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-(bromomethyl)-1-(2,3,4,6-tetra-O-acetylhexopyranosyl)-1H-1,2,3-triazole

There total 2 articles about 4-(bromomethyl)-1-(2,3,4,6-tetra-O-acetylhexopyranosyl)-1H-1,2,3-triazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

propargyl bromide (106-96-7) + 1-azido-1-deoxy-β-D-glucopyranoside tetraacetate (13992-25-1) → 4-bromomethyl-1-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-1,2,3-triazole (70380-26-6)

Guidance literature:

With copper(II) sulphate hydrate; sodium L-ascorbate; In water; tert-butyl alcohol; at 20 ℃; for 16h;

DOI:10.1016/j.carres.2014.10.009

Reference yield:

→ 4-bromomethyl-1-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-1,2,3-triazole (70380-26-6)

Guidance literature:

Tetraacetyl-glucosylazid, Propargylbromid;

DOI:10.1021/jm00191a007

upstream raw materials:

propargyl bromide

1-azido-1-deoxy-β-D-glucopyranoside tetraacetate

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