Base Information
- Chemical Name:3H-tetrazolo[5,1-i]purine
- CAS No.:211-42-7
- Molecular Formula:C5H3N7
- Molecular Weight:161.1242
- Hs Code.:
- Mol file:211-42-7.mol
Synonyms:
Synonyms:
98% *data from raw suppliers
There total 1 articles about 3H-tetrazolo[5,1-i]purine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
Reference yield:
The research describes practical procedures for synthesizing selectively protected a-aminosuberic acid and a,a'-diaminosuberic acid using mixed Kolbe electrolytic decarboxylative dimerization of different carboxylic acids. The purpose of the study is to develop a method for creating these intermediates, which are useful in the preparation of dicarba and desaminodicarba analogues of cystine peptides, known for their high biological activity and enhanced stability due to the absence of reducible disulfide linkages. The key chemicals used include a-tert-butyl N-Boc-L-glutamate (2a), a-methyl N-Cbz-L-glutamate (1), a-tert-butyl N-Boc-D-glutamate (2b), and methyl glutarate (8). The study concludes that by using readily available selectively blocked glutamic acid derivatives and incorporating desired protecting groups and stereochemistry prior to Kolbe dimerization, the desired unsymmetrical dimers can be isolated without racemization of chiral centers. The method provides a practical and efficient way to synthesize optically pure, selectively protected diamino- and monoamino suberic acid derivatives for use in peptide synthesis.
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