3-methylbenzaldehyde (3-methylbenzylidene)hydrazone

Base Information

• Chemical Name: 3-methylbenzaldehyde (3-methylbenzylidene)hydrazone
• CAS No.: 58896-23-4
• Molecular Formula: C16H16N2
• Molecular Weight: 236.316
• Mol file: 58896-23-4.mol

Synonyms:3,3'-dimethylbenzalazine;N,N'-Bis-[1-m-tolyl-meth-(E)-ylidene]-hydrazine;3,3'-Dimethyl-benzaldazin;bis-(3-methyl-benzylidene)-hydrazine;Bis-(3-methyl-benzyliden)-hydrazin;

Chemical Property of 3-methylbenzaldehyde (3-methylbenzylidene)hydrazone

Chemical Property:

• PSA: 24.72000
• LogP: 3.75640

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-methylbenzaldehyde (3-methylbenzylidene)hydrazone

There total 6 articles about 3-methylbenzaldehyde (3-methylbenzylidene)hydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

m-tolyl aldehyde (620-23-5) → 3,3'-dimethylbenzaldazine (58896-23-4)

Guidance literature:

With hydrazine hydrochloride; ethanol; water;

Reference yield:

m-tolyl aldehyde (620-23-5) → N,N'-Bis-[1-m-tolyl-meth-(E)-ylidene]-hydrazine (58896-23-4)

Guidance literature:

With hydrazine hydrate; acetic acid; In ethanol; at 100 ℃; for 10h;

DOI:10.1021/acs.joc.7b01472

Reference yield:

m-tolyldiazomethane (40154-67-4) → (E)-3,3'-dimethylstilbene (35286-92-1) + cis-3,3'-dimethylstilbene (20657-32-3) + N,N'-Bis-[1-m-tolyl-meth-(E)-ylidene]-hydrazine (58896-23-4)

Guidance literature:

copper(II) perchlorate; In acetonitrile; at 20 ℃; for 0.2h; Yield given;

DOI:10.1246/cl.1985.1895

upstream raw materials:

m-tolyl aldehyde

3-Methylbenzonitrile

m-tolyldiazomethane

Downstream raw materials:

2-(3-methylbenzylidene)hydrazinocarbothioamide

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