3,4-Dimethoxyfuran

Base Information

• Chemical Name: 3,4-Dimethoxyfuran
• CAS No.: 58928-51-1
• Molecular Formula: C6H8O3
• Molecular Weight: 128.128
• DSSTox Substance ID: DTXSID40496185
• Nikkaji Number: J897.861A
• Wikidata: Q82344884
• Mol file: 58928-51-1.mol

Synonyms:3,4-dimethoxyfuran;58928-51-1;SCHEMBL2762009;DTXSID40496185

Chemical Property of 3,4-Dimethoxyfuran

Chemical Property:

• XLogP3: 0.9
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 2
• Exact Mass: 128.047344113
• Heavy Atom Count: 9
• Complexity: 74.4

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: COC1=COC=C1OC

Technology Process of 3,4-Dimethoxyfuran

There total 4 articles about 3,4-Dimethoxyfuran which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(1S,2R,7S,8R)-9,10-Dimethoxy-4-methyl-11-oxa-tricyclo[6.2.1.02,7]undeca-4,9-diene-3,6-dione (72826-56-3,85956-27-0,93301-70-3) → 3,4-dimethoxyfuran (58928-51-1) + 2-Methyl-1,4-benzoquinone (553-97-9)

Guidance literature:

In chloroform-d1; at 25.9 ℃; Rate constant; Thermodynamic data; activation energie (Ea), other temperatures;

DOI:10.1021/jo00207a035

Reference yield:

5,6-dimethoxy-2endo,3endo-dimethyl-7-oxabicyclo<2.2.1>hept-5-ene-2,3-dicarboxylic anhydride (82616-93-1) → 2,3-Dimethylmaleic anhydride (766-39-2) + 3,4-dimethoxyfuran (58928-51-1)

Guidance literature:

In chloroform; Ambient temperature;

DOI:10.1002/hlca.19820650332

Reference yield:

7,10-epoxy-8,9-dimethoxy-cis-1-transoid-1,10-cis-10-bicyclo<4.4.0>deca-3,8-dien-2,5-dione (72880-96-7) → 3,4-dimethoxyfuran (58928-51-1) + p-benzoquinone (106-51-4)

Guidance literature:

In chloroform-d1; at 25.9 ℃; Rate constant; Thermodynamic data; activation energie (Ea), other temperatures;

DOI:10.1021/jo00207a035

upstream raw materials:

7,10-epoxy-8,9-dimethoxy-cis-1-transoid-1,10-cis-10-bicyclo<4.4.0>deca-3,8-dien-2,5-dione

(1S,2R,7S,8R)-9,10-Dimethoxy-4-methyl-11-oxa-tricyclo[6.2.1.0^2,7]undeca-4,9-diene-3,6-dione

(1R,2S,7R,8S)-4,5,9,10-Tetramethoxy-11-oxa-tricyclo[6.2.1.0^2,7]undeca-4,9-diene-3,6-dione

5,6-dimethoxy-2endo,3endo-dimethyl-7-oxabicyclo<2.2.1>hept-5-ene-2,3-dicarboxylic anhydride

Downstream raw materials:

3,4-dimethoxy-5-(1-(benzyloxy)ethyl)-2-furaldehyde

2-(1-(benzyloxy)ethyl)-3,4-dimethoxyfuran

2,3-dimethoxy-5-methyl-6-phenylphenol

1,7-dimethyl-2,6-diphenyl-4-oxaspiro[2.4]hepta-1,6-dien-5-one