Technology Process of 4(3H)-Quinazolinone, 7-amino-3-(phenylmethyl)-
There total 5 articles about 4(3H)-Quinazolinone, 7-amino-3-(phenylmethyl)- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
ammonium formate;
palladium on activated charcoal;
In
ethanol;
at 65 ℃;
for 0.166667h;
microwave irradiation;
DOI:10.1016/S0040-4039(03)01026-8
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 86 percent / 0.67 h / 150 °C / microwave irradiation
2: 80 percent / NaH / dimethylformamide / 0.25 h / 70 °C / microwave irradiation
3: 75 percent / ammonium formate / Pd/C / ethanol / 0.17 h / 65 °C / microwave irradiation
With
ammonium formate; sodium hydride;
palladium on activated charcoal;
In
ethanol; N,N-dimethyl-formamide;
1: Niementowski condensation;
DOI:10.1016/S0040-4039(03)01026-8
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 80 percent / NaH / dimethylformamide / 0.25 h / 70 °C / microwave irradiation
2: 75 percent / ammonium formate / Pd/C / ethanol / 0.17 h / 65 °C / microwave irradiation
With
ammonium formate; sodium hydride;
palladium on activated charcoal;
In
ethanol; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(03)01026-8
