4-((9H-Fluoren-9-ylidene)methyl)-N,N-dimethylaniline

Base Information

Chemical Name:4-((9H-Fluoren-9-ylidene)methyl)-N,N-dimethylaniline
CAS No.:2871-86-5
Molecular Formula:C22H19 N
Molecular Weight:297.4
Hs Code.:
Mol file:2871-86-5.mol

Synonyms:p-Toluidine,a-fluoren-9-ylidene-N,N-dimethyl-(6CI,7CI,8CI); 9-(4'-Dimethylaminobenzylidene)fluorene; 9-(p-Dimethylamino)benzylidenefluorene;NSC 12314; NSC 92066

Suppliers and Price of 4-((9H-Fluoren-9-ylidene)methyl)-N,N-dimethylaniline

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
4-((9H-Fluoren-9-ylidene)methyl)-N,N-dimethylaniline 95+%
1g
$ 581.00

American Custom Chemicals Corporation
9-(4-(DIMETHYLAMINO)BENZYLIDENE)FLUORENE 95.00%
10G
$ 1222.00

American Custom Chemicals Corporation
9-(4-(DIMETHYLAMINO)BENZYLIDENE)FLUORENE 95.00%
5G
$ 866.27

American Custom Chemicals Corporation
9-(4-(DIMETHYLAMINO)BENZYLIDENE)FLUORENE 95.00%
1G
$ 626.43

Alichem
4-((9H-Fluoren-9-ylidene)methyl)-N,N-dimethylaniline
1g
$ 511.92

Total 7 raw suppliers

Chemical Property of 4-((9H-Fluoren-9-ylidene)methyl)-N,N-dimethylaniline

Chemical Property:

Vapor Pressure:1.53E-08mmHg at 25°C
Boiling Point:457.1°Cat760mmHg
Flash Point:182.9°C
PSA：3.24000
Density:1.17g/cm³
LogP:5.32190
Storage Temp.:2-8°C

Purity/Quality:

99% ^*data from raw suppliers

4-((9H-Fluoren-9-ylidene)methyl)-N,N-dimethylaniline 95+% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Uses 9-(4-(Dimethylamino)Benzylidene)Fluorene is used in preparation of dispiroheterocycles through solvent-free microwave-assisted [3+2] cycloaddition of azomethine ylides with 9-arylidenefluorenes.

Technology Process of 4-((9H-Fluoren-9-ylidene)methyl)-N,N-dimethylaniline

There total 9 articles about 4-((9H-Fluoren-9-ylidene)methyl)-N,N-dimethylaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 13379-29-8
2-bromo-2'-(bromomethyl)-1,1'-biphenyl

: 18708-16-2
p-(dimethylamino)benzaldehyde tosylhydrazone

: 2871-86-5
4-((9H-fluoren-9-ylidene)methyl)-N,N-dimethylaniline

Guidance literature:: With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; trifuran-2-yl-phosphane; caesium carbonate; lithium tert-butoxide; In 1,4-dioxane; at 120 ℃; for 12h; Inert atmosphere; Sealed tube;
DOI:10.1021/acs.orglett.7b00613