4-[2-(4-Bromo-2,6-dimethylphenoxy)ethoxy]-3-methoxybenzaldehyde

Base Information

• Chemical Name: 4-[2-(4-Bromo-2,6-dimethylphenoxy)ethoxy]-3-methoxybenzaldehyde
• CAS No.: 6450-19-7
• Molecular Formula: C19H14 Cl2 N2
• Molecular Weight: 341.24
• DSSTox Substance ID: DTXSID60367747
• Wikidata: Q82153794

Synonyms:4-[2-(4-bromo-2,6-dimethylphenoxy)ethoxy]-3-methoxybenzaldehyde;6450-19-7;DTXSID60367747;AKOS001360368;EN300-1188700;Z237482726;428462-64-0

Chemical Property of 4-[2-(4-Bromo-2,6-dimethylphenoxy)ethoxy]-3-methoxybenzaldehyde

Chemical Property:

• Vapor Pressure: 3.37E-10mmHg at 25°C
• Boiling Point: 501.8°Cat760mmHg
• Flash Point: 257.3°C
• Density: 1.341g/cm³
• XLogP3: 4.4
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 7
• Exact Mass: 378.04667
• Heavy Atom Count: 23
• Complexity: 353

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC1=CC(=CC(=C1OCCOC2=C(C=C(C=C2)C=O)OC)C)Br

Technology Process of 4-[2-(4-Bromo-2,6-dimethylphenoxy)ethoxy]-3-methoxybenzaldehyde

There total 3 articles about 4-[2-(4-Bromo-2,6-dimethylphenoxy)ethoxy]-3-methoxybenzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

5,5,6,6-tetrafluoro-cyclohepta-1,3-diene (2267-32-5) + 4-chloro-aniline (106-47-8) → 1-<4-Chlorphenyl-amino>-7-<4-chlorphenyl-imino>-1,3,5-cycloheptatrien (6450-19-7)

Guidance literature:

With triethylamine;

DOI:10.1021/ja01475a031

Reference yield:

{Ni(ClC6H4NC7H5NC6H4Cl)2} (14444-89-4) + 2-ethylamino-tropone-ethylimine (3602-29-7) → 2-{4-chloro-phenylamino}-tropone-{4-chloro-phenylimine} (6450-19-7) + {Ni(C6H4ClNC7H5NC6H4Cl)(C2H5NC7H5NC2H5)} (14726-27-3)

Guidance literature:

DOI:10.1063/1.1696756

Reference yield:

→ 1-<4-Chlorphenyl-amino>-7-<4-chlorphenyl-imino>-1,3,5-cycloheptatrien (6450-19-7)

Guidance literature:

1,1,2,2-Tetrafluor-cycloheptadien-(3,5), p-Chloranilin;

DOI:10.1021/ja01489a055

upstream raw materials:

5,5,6,6-tetrafluoro-cyclohepta-1,3-diene

4-chloro-aniline

{Ni(ClC₆H₄NC₇H₅NC₆H₄Cl)2}

2-ethylamino-tropone-ethylimine

Downstream raw materials:

N-(4-chlorophenyl)-2-aminotropone

1-<4-Chlorphenyl-amino>-4-brom-7-<4-chlorphenyl-imino>-1,3,5-cycloheptatrien

{Ni(ClC₆H₄NC₇H₅NC₆H₄Cl)2}

{Ni(C₆H₄ClNC₇H₅NC₆H₄Cl)(C₂H₅NC₇H₄(FC₆H₄NN)NC₂H₅)}

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