2-Amino-5-methoxy-3-nitrobenzene-1-thiol

Base Information

Chemical Name:2-Amino-5-methoxy-3-nitrobenzene-1-thiol
CAS No.:59334-05-3
Molecular Formula:C7H8N2O3S
Molecular Weight:200.21500
Hs Code.:2930909090
DSSTox Substance ID:DTXSID10506861
Wikidata:Q82362819

Synonyms:59334-05-3;2-Amino-5-methoxy-3-nitrobenzene-1-thiol;DTXSID10506861

Suppliers and Price of 2-Amino-5-methoxy-3-nitrobenzene-1-thiol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 0 raw suppliers

Chemical Property of 2-Amino-5-methoxy-3-nitrobenzene-1-thiol

Chemical Property:

PSA：119.87000
LogP:2.57870
XLogP3:1.7
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:1
Exact Mass:200.02556330
Heavy Atom Count:13
Complexity:197

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=CC(=C(C(=C1)S)N)[N+](=O)[O-]

Technology Process of 2-Amino-5-methoxy-3-nitrobenzene-1-thiol

There total 3 articles about 2-Amino-5-methoxy-3-nitrobenzene-1-thiol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 203387-16-0
2-Chloro-6-methoxy-4-nitro-2λ⁴-benzo[1,2,3]dithiazole

: 59334-05-3
5-methoxy-3-nitro-2-aminobenzenethiol

Guidance literature:: With sodium hydroxide; sodium hydrogensulfite; In water; for 5h; Heating;

Reference yield:

: 59334-05-3
5-methoxy-3-nitro-2-aminobenzenethiol

Guidance literature:: With sodium hydroxide; sodium dithionite;
DOI:10.1021/ja01212a066 DOI:10.1021/ja01877a019

Reference yield:

: 96-96-8
4-methoxy-2-nitroaniline

: 59334-05-3
5-methoxy-3-nitro-2-aminobenzenethiol

Guidance literature:: Multi-step reaction with 2 steps

1: sulphur monochloride / acetic acid / 1) 0-10 deg C, 2) room temperature, 0.5 h, 3) 70 deg C, 5 h, 4) 90 deg C

2: 63 percent / sodium hydroxide, sodium bisulphite / H₂O / 5 h / Heating

With sodium hydroxide; sulfur dichloride; sodium hydrogensulfite; In water; acetic acid;