o-(4-Diethylamino-2-methoxybenzoyl)benzoic acid

Base Information

Chemical Name:o-(4-Diethylamino-2-methoxybenzoyl)benzoic acid
CAS No.:59404-96-5
Molecular Formula:C19H21NO4
Molecular Weight:327.38
Hs Code.:
Mol file:59404-96-5.mol

Synonyms:

Suppliers and Price of o-(4-Diethylamino-2-methoxybenzoyl)benzoic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 3 raw suppliers

Chemical Property of o-(4-Diethylamino-2-methoxybenzoyl)benzoic acid

Chemical Property:

Boiling Point:546.6±50.0 °C(Predicted)
PKA:3.29±0.36(Predicted)
PSA：66.84000
Density:1.190±0.06 g/cm3(Predicted)
LogP:3.47060

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of o-(4-Diethylamino-2-methoxybenzoyl)benzoic acid

There total 1 articles about o-(4-Diethylamino-2-methoxybenzoyl)benzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 85-44-9
phthalic anhydride

: 92-18-2
N,N-diethyl-3-methoxyaniline

: 59404-96-5
4-diethylamino-2-methoxy-2'-carboxybenzophenone

Guidance literature:: phthalic anhydride; N,N-diethyl-3-methoxyaniline; With aluminum (III) chloride; In dichloromethane; at 0 ℃; for 4h; Inert atmosphere;

With hydrogenchloride; water; In dichloromethane; for 0.166667h; Inert atmosphere;
DOI:10.1039/c0cc03407j

Reference yield: 65.0%

: 59404-96-5
4-diethylamino-2-methoxy-2'-carboxybenzophenone

: 5809-23-4
2'-Carboxy-4-diethylamino-2-hydroxybenzophenon

Guidance literature:: 4-diethylamino-2-methoxy-2'-carboxybenzophenone; With boron tribromide; In dichloromethane; at -78 - -25 ℃;

With water; In dichloromethane;
DOI:10.1039/c0cc03407j

Reference yield:

: 59404-96-5
4-diethylamino-2-methoxy-2'-carboxybenzophenone

: C₄₂H₃₈N₂O₆⁽²⁺⁾

Guidance literature:: Multi-step reaction with 3 steps

1.1: boron tribromide / dichloromethane / -78 - -25 °C

2.1: methanesulfonic acid / 2 h / 90 °C / Sealed tube

2.2: 0.33 h / pH 11 - 12 / Cooling with ice

3.1: trifluoroacetic acid / tetrahydrofuran

With methanesulfonic acid; boron tribromide; trifluoroacetic acid; In tetrahydrofuran; dichloromethane;