2-bromo-2,3-dimethylbutane

Base Information

• Chemical Name: 2-bromo-2,3-dimethylbutane
• CAS No.: 594-52-5
• Molecular Formula: C6H13Br
• Molecular Weight: 165.073
• Mol file: 594-52-5.mol

Synonyms:thexyl bromide;2-Brom-2,3-dimethyl-butan;NILGDLGIGRGWRL-UHFFFAOYSA;Butane,2-bromo-2,3-dimethyl;Butane, 2-bromo-2,3-dimethyl-;InChI=1/C6H13Br/c1-5(2)6(3,4)7/h5H,1-4H3;Pinakolinalkohol-bromid;2-bromo-2,3-dimethyl-butane;

Chemical Property of 2-bromo-2,3-dimethylbutane

Chemical Property:

• Melting Point: 25°C
• Refractive Index: 1.4507
• Boiling Point: 147.26°C (estimate)
• PSA: 0.00000
• Density: 1.1804
• LogP: 2.81590

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-bromo-2,3-dimethylbutane

There total 3 articles about 2-bromo-2,3-dimethylbutane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

2,3-Dimethyl-2-butene (563-79-1) + {PtBr4} (16893-18-8,16893-21-3) → cis-dichloro-bis-triethylphosphine platinum(II) (15692-84-9,13985-90-5,15636-78-9) + trans-PtBr2(triethylphosphine)2 (15692-84-9,15636-78-9,13985-90-5) + 2,3-dibromo-2,3-dimethylbutane (594-81-0) + 2-bromo-2,3-dimethylbutane (594-52-5) + 1-bromo-2,3-dimethyl-2-butene (5072-70-8)

Guidance literature:

In chloroform-d1; Concentration; Photolysis; Inert atmosphere;

DOI:10.1021/ic4004998

Reference yield: 0.57%

2,3-dimethylbutane (79-29-8) → 2-bromo-2,3-dimethylbutane (594-52-5) + 1-bromo-2,3-dimethyl-butane (30540-31-9)

Guidance literature:

With 2-Picolinic acid; Bromotrichloromethane; dihydrogen peroxide; relative reactivity;

DOI:10.1016/S0040-4039(00)94704-X

Reference yield:

2,3-dimethylbutane (79-29-8) → 2,3-dibromo-2,3-dimethylbutane (594-81-0) + 1,4-dibromo-2,3-dimethyl-but-2-ene (34619-20-0) + 2-bromo-2,3-dimethylbutane (594-52-5)

Guidance literature:

at 100 ℃; Photobromierung in der Dampfphase;

DOI:10.1021/jo01123a021

upstream raw materials:

2,3-dimethylbutane

2,3-Dimethyl-2-butene

{PtBr4}

Downstream raw materials:

2,3-Dimethyl-2-butene

2,3-dimethylbutan-2-ol

2,3-dibromo-2,3-dimethylbutane

2,3-Dimethyl-1-butene