N-(3-Methylbutanoyl)-L-valyl-L-valine

Base Information

Chemical Name:N-(3-Methylbutanoyl)-L-valyl-L-valine
CAS No.:59452-57-2
Molecular Formula:C15H28N2O4
Molecular Weight:300.398
Hs Code.:
DSSTox Substance ID:DTXSID40561660
Nikkaji Number:J1.382.688I
Wikidata:Q82445505

Synonyms:59452-57-2;N-(3-Methylbutanoyl)-L-valyl-L-valine;isovaleryl-l-valyl-l-valine;DTXSID40561660

Suppliers and Price of N-(3-Methylbutanoyl)-L-valyl-L-valine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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Total 0 raw suppliers

Chemical Property of N-(3-Methylbutanoyl)-L-valyl-L-valine

Chemical Property:

XLogP3:1.6
Hydrogen Bond Donor Count:3
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:8
Exact Mass:300.20490738
Heavy Atom Count:21
Complexity:378

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(C)CC(=O)NC(C(C)C)C(=O)NC(C(C)C)C(=O)O
Isomeric SMILES:CC(C)CC(=O)N[C@@H](C(C)C)C(=O)N[C@@H](C(C)C)C(=O)O

Technology Process of N-(3-Methylbutanoyl)-L-valyl-L-valine

There total 1 articles about N-(3-Methylbutanoyl)-L-valyl-L-valine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 3918-94-3
Val-Val

: 108-12-3
isopentanoyl chloride

: 59452-57-2
N-isovaleryl-L-valyl-L-valine

Guidance literature:: With sodium hydroxide;
DOI:10.1016/S0040-4020(01)00543-9

Reference yield: 65.0%

: 59452-57-2
N-isovaleryl-L-valyl-L-valine

: 306314-20-5
(3S,4R)-4-[(S)-2-((3S,4R)-4-Amino-5,5,5-trifluoro-3-hydroxy-pentanoylamino)-propionylamino]-5,5,5-trifluoro-3-hydroxy-pentanoic acid methyl ester

: 306314-21-6
(3S,4R)-5,5,5-Trifluoro-3-hydroxy-4-[(S)-2-((3S,4R)-5,5,5-trifluoro-3-hydroxy-4-{(S)-3-methyl-2-[(S)-3-methyl-2-(3-methyl-butyrylamino)-butyrylamino]-butyrylamino}-pentanoylamino)-propionylamino]-pentanoic acid methyl ester

Guidance literature:: With 4-methyl-morpholine; isobutyl chloroformate; In ethyl acetate; at 20 ℃; for 96h;
DOI:10.1016/S0040-4039(00)01244-2

Reference yield:

: 59452-57-2
N-isovaleryl-L-valyl-L-valine

: H2N-HiSta(?-BOM)-OMe*HCl

: 120849-35-6
(3S,4R)-5-(3-Benzyloxymethyl-3H-imidazol-4-yl)-3-hydroxy-4-{(S)-3-methyl-2-[(S)-3-methyl-2-(3-methyl-butyrylamino)-butyrylamino]-butyrylamino}-pentanoic acid methyl ester

: 120742-10-1
N-Isovaleryl-L-Valyl-L-Valyl-4(S)-amino-5-<3-(benzyloxymethyl)imidazol-4-yl>-3(S)-hydroxypentanoic Acid Methyl Ester

Guidance literature:: With benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide; Yield given. Multistep reaction; 1.) CH₂Cl₂, DMF, 0 deg C, 2 h, 2 a.) 0 deg C, 3 h, 2 b.) r.t., overnight;
DOI:10.1021/jm00127a028