2-Azetidinone, 3-(4-pentenyl)-1-(phenylmethoxy)-, (3R)-

Base Information

Chemical Name:2-Azetidinone, 3-(4-pentenyl)-1-(phenylmethoxy)-, (3R)-
CAS No.:596111-57-8
Molecular Formula:C15H19NO2
Molecular Weight:245.321
Hs Code.:

Synonyms:

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Chemical Property of 2-Azetidinone, 3-(4-pentenyl)-1-(phenylmethoxy)-, (3R)-

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Technology Process of 2-Azetidinone, 3-(4-pentenyl)-1-(phenylmethoxy)-, (3R)-

There total 6 articles about 2-Azetidinone, 3-(4-pentenyl)-1-(phenylmethoxy)-, (3R)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 596111-56-7
N-benzyloxy-2R-hydroxymethyl-6-heptenamide

: 596111-57-8
N-benzyloxy-α-(4-penten-1-yl)-β-lactam

Guidance literature:: With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; at 20 ℃;
DOI:10.1021/jm034113f

Reference yield:

: 21430-12-6
6-heptenoyl chloride

: 596111-57-8
N-benzyloxy-α-(4-penten-1-yl)-β-lactam

Guidance literature:: Multi-step reaction with 5 steps

1: 9.55 g / LiCl / tetrahydrofuran / 6 h

2: 52 percent / TiCl₄; diisopropylethylamine / CH₂Cl₂ / 2 h

3: aq. H₂O₂; LiOH / tetrahydrofuran / 2 h

4: Et₃N; HBTU / acetonitrile / 3 h

5: 88 percent / triphenylphosphine; diisopropyl azodicarboxylate / tetrahydrofuran / 20 °C

With lithium hydroxide; di-isopropyl azodicarboxylate; dihydrogen peroxide; titanium tetrachloride; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine; N-ethyl-N,N-diisopropylamine; triphenylphosphine; lithium chloride; In tetrahydrofuran; dichloromethane; acetonitrile; 5: Mitsunobu reaction;
DOI:10.1021/jm034113f

Reference yield:

: 1119-60-4
hept-6-enoic acid

: 596111-57-8
N-benzyloxy-α-(4-penten-1-yl)-β-lactam

Guidance literature:: Multi-step reaction with 6 steps

1: Et₃N; pivaloyl chloride / tetrahydrofuran / 1 h

2: 9.55 g / LiCl / tetrahydrofuran / 6 h

3: 52 percent / TiCl₄; diisopropylethylamine / CH₂Cl₂ / 2 h

4: aq. H₂O₂; LiOH / tetrahydrofuran / 2 h

5: Et₃N; HBTU / acetonitrile / 3 h

6: 88 percent / triphenylphosphine; diisopropyl azodicarboxylate / tetrahydrofuran / 20 °C

With lithium hydroxide; di-isopropyl azodicarboxylate; dihydrogen peroxide; pivaloyl chloride; titanium tetrachloride; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine; N-ethyl-N,N-diisopropylamine; triphenylphosphine; lithium chloride; In tetrahydrofuran; dichloromethane; acetonitrile; 6: Mitsunobu reaction;
DOI:10.1021/jm034113f