Benzene, 1-(1-bromopropyl)-4-(2-methylpropyl)-

Base Information

Chemical Name:Benzene, 1-(1-bromopropyl)-4-(2-methylpropyl)-
CAS No.:59771-03-8
Molecular Formula:C13H19Br
Molecular Weight:255.198
Hs Code.:
DSSTox Substance ID:DTXSID90449762

Synonyms:Benzene, 1-(1-bromopropyl)-4-(2-methylpropyl)-;59771-03-8;SCHEMBL8123426;DTXSID90449762;JLLGMLODKYNBKJ-UHFFFAOYSA-N;1-bromo-1-(4-isobutylphenyl)propane;AKOS012743125

Suppliers and Price of Benzene, 1-(1-bromopropyl)-4-(2-methylpropyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzene, 1-(1-bromopropyl)-4-(2-methylpropyl)-

Chemical Property:

XLogP3:5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:4
Exact Mass:254.06701
Heavy Atom Count:14
Complexity:145

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCC(C1=CC=C(C=C1)CC(C)C)Br

Technology Process of Benzene, 1-(1-bromopropyl)-4-(2-methylpropyl)-

There total 4 articles about Benzene, 1-(1-bromopropyl)-4-(2-methylpropyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.7%

: 59770-94-4,185062-54-8
1-(4-isobutylphenyl)propan-1-ol

: 59771-03-8
1-bromo-1-(4-isobutylphenyl)propane

Guidance literature:: With carbon tetrabromide; triphenylphosphine; In tetrahydrofuran; at 20 ℃; for 5h;
DOI:10.1248/cpb.49.799

Reference yield:

: 59771-24-3
4-isobutylpropiophenone

: 59771-03-8
1-bromo-1-(4-isobutylphenyl)propane

Guidance literature:: Multi-step reaction with 2 steps

1: 99.2 percent / NaBH₄ / methanol / 1 h / 20 °C

2: 35.7 percent / CBr₄; PPh₃ / tetrahydrofuran / 5 h / 20 °C

With sodium tetrahydroborate; carbon tetrabromide; triphenylphosphine; In tetrahydrofuran; methanol;
DOI:10.1248/cpb.49.799

Reference yield:

: 538-93-2
1-phenyl-2-methylpropane

: 59771-03-8
1-bromo-1-(4-isobutylphenyl)propane

Guidance literature:: Multi-step reaction with 3 steps

1.1: AlCl₃ / CH₂Cl₂ / 0.5 h / 0 °C

1.2: 99.2 percent / CH₂Cl₂ / 1 h / 0 °C

2.1: 99.2 percent / NaBH₄ / methanol / 1 h / 20 °C

3.1: 35.7 percent / CBr₄; PPh₃ / tetrahydrofuran / 5 h / 20 °C

With sodium tetrahydroborate; aluminium trichloride; carbon tetrabromide; triphenylphosphine; In tetrahydrofuran; methanol; dichloromethane; 1.2: Friedel-Crafts acylation;
DOI:10.1248/cpb.49.799