1,4-Benzodioxin, 2,3-dihydro-5,7-dinitro-

Base Information

Chemical Name:1,4-Benzodioxin, 2,3-dihydro-5,7-dinitro-
CAS No.:59820-95-0
Molecular Formula:C8H6N2O6
Molecular Weight:226.145
Hs Code.:
DSSTox Substance ID:DTXSID70481549
Nikkaji Number:J406.143H
Wikidata:Q82317023

Synonyms:59820-95-0;1,4-Benzodioxin, 2,3-dihydro-5,7-dinitro-;DTXSID70481549

Suppliers and Price of 1,4-Benzodioxin, 2,3-dihydro-5,7-dinitro-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,4-Benzodioxin, 2,3-dihydro-5,7-dinitro-

Chemical Property:

XLogP3:1.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:0
Exact Mass:226.02258592
Heavy Atom Count:16
Complexity:298

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1COC2=C(C=C(C=C2O1)[N+](=O)[O-])[N+](=O)[O-]

Technology Process of 1,4-Benzodioxin, 2,3-dihydro-5,7-dinitro-

There total 4 articles about 1,4-Benzodioxin, 2,3-dihydro-5,7-dinitro- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 14.0%

: 57356-28-2
5-nitro-2,3-dihydro-1,4-benzodioxin

: 59820-94-9
5,6-dinitro-2,3-dihydrobenzo[b][1,4]dioxine

: 59820-95-0
5,7-dinitro-2,3-dihydro-benzo[1,4]dioxine

Guidance literature:: With nitric acid; acetic acid; at 25 ℃; for 0.5h;

Reference yield: 3.0%

: 16498-20-7
6-nitro-2,3-dihydrobenzo[b][1,4]dioxine

: 57356-48-6
6,7-dinitro-2,3-dihydrobenzo[1,4]dioxine

: 59820-94-9
5,6-dinitro-2,3-dihydrobenzo[b][1,4]dioxine

: 59820-95-0
5,7-dinitro-2,3-dihydro-benzo[1,4]dioxine

Guidance literature:: With nitric acid; acetic acid; at 25 ℃; for 0.5h; Title compound not separated from byproducts;

Reference yield:

: 6665-98-1
3-nitrobenzene-1,2-diol

: 59820-95-0
5,7-dinitro-2,3-dihydro-benzo[1,4]dioxine

Guidance literature:: Multi-step reaction with 2 steps

1: 74 percent / anh. potassium carbonate / 3-methyl-butan-1-ol / 1.) reflux, 7 h 2.) reflux, 8 h

2: 14 percent / glacial acetic acid, fuming nitric acid / 0.5 h / 25 °C

With nitric acid; potassium carbonate; acetic acid; In i-Amyl alcohol;