5-Amino-6-nitroisoindoline-1,3-dione

Base Information

Chemical Name:5-Amino-6-nitroisoindoline-1,3-dione
CAS No.:59827-85-9
Molecular Formula:C8H5N3O4
Molecular Weight:207.145
Hs Code.:
DSSTox Substance ID:DTXSID90569010
Nikkaji Number:J1.061.945I
Wikidata:Q82455703

Synonyms:5-amino-6-nitroisoindoline-1,3-dione;59827-85-9;5-amino-6-nitroisoindole-1,3-dione;5-Amino-6-nitro-1H-isoindole-1,3(2H)-dione;4-Amino-5-nitrophthalimide;SCHEMBL438741;DTXSID90569010;JOPWCYFGRYCBEF-UHFFFAOYSA-N;MFCD13186915;5-Amino-6-nitro-isoindole-1,3-dione;SB64931;BP-10502;CS-0197309;E73982

Suppliers and Price of 5-Amino-6-nitroisoindoline-1,3-dione

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 13 raw suppliers

Chemical Property of 5-Amino-6-nitroisoindoline-1,3-dione

Chemical Property:

XLogP3:0.4
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:0
Exact Mass:207.02800565
Heavy Atom Count:15
Complexity:337

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=C2C(=CC(=C1N)[N+](=O)[O-])C(=O)NC2=O

Technology Process of 5-Amino-6-nitroisoindoline-1,3-dione

There total 5 articles about 5-Amino-6-nitroisoindoline-1,3-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 6015-57-2
5-chloro-6-nitroisoindole-1,3-dione

: 59827-85-9
5-amino-6-nitroisoindoline-1,3-dione

Guidance literature:: With urea; at 150 ℃; for 6h;

Reference yield:

: 89-40-7
4-nitrophthalimide

: 59827-85-9
5-amino-6-nitroisoindoline-1,3-dione

Guidance literature:: Multi-step reaction with 4 steps

1.1: tin(ll) chloride; hydrogenchloride / water / 2 h / 50 °C

2.1: hydrogenchloride; sodium nitrite / water / 1 h / 0 °C

2.2: 4 h / 0 - 50 °C

3.1: sulfuric acid; nitric acid / 0.5 h / 80 °C

4.1: urea; copper(II) sulfate / formamide / 140 °C

With hydrogenchloride; sulfuric acid; nitric acid; copper(II) sulfate; urea; tin(ll) chloride; sodium nitrite; In water; formamide;
DOI:10.1016/j.cclet.2017.09.015

Reference yield:

: 136918-14-4,85-41-6
phthalimide

: 59827-85-9
5-amino-6-nitroisoindoline-1,3-dione

Guidance literature:: Multi-step reaction with 5 steps

1.1: sulfuric acid; nitric acid / 1 h / 80 °C

2.1: tin(ll) chloride; hydrogenchloride / water / 2 h / 50 °C

3.1: hydrogenchloride; sodium nitrite / water / 1 h / 0 °C

3.2: 4 h / 0 - 50 °C

4.1: sulfuric acid; nitric acid / 0.5 h / 80 °C

5.1: urea; copper(II) sulfate / formamide / 140 °C

With hydrogenchloride; sulfuric acid; nitric acid; copper(II) sulfate; urea; tin(ll) chloride; sodium nitrite; In water; formamide;
DOI:10.1016/j.cclet.2017.09.015