Cyclohexanol, 1-(1-nitropropyl)-

Base Information

• Chemical Name: Cyclohexanol, 1-(1-nitropropyl)-
• CAS No.: 59906-63-7
• Molecular Formula: C9H17NO3
• Molecular Weight: 187.239
• DSSTox Substance ID: DTXSID90444994
• Nikkaji Number: J1.135.115H
• Mol file: 59906-63-7.mol

Synonyms:Cyclohexanol, 1-(1-nitropropyl)-;59906-63-7;1-(1-Nitropropyl)cyclohexanol;DTXSID90444994

Chemical Property of Cyclohexanol, 1-(1-nitropropyl)-

Chemical Property:

• XLogP3: 2.5
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 2
• Exact Mass: 187.12084340
• Heavy Atom Count: 13
• Complexity: 182

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCC(C1(CCCCC1)O)[N+](=O)[O-]

Technology Process of Cyclohexanol, 1-(1-nitropropyl)-

There total 2 articles about Cyclohexanol, 1-(1-nitropropyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

cyclohexanone (108-94-1,11119-77-0,9003-41-2,9075-99-4) + 1-Nitropropane (108-03-2) → 1-(1-Nitro-propyl)-cyclohexanol (59906-63-7)

Guidance literature:

With P(i-PrNCH₂CH₂)3N; magnesium sulfate; for 7h; Ambient temperature;

DOI:10.1021/jo9818733

Reference yield:

→ 1-(1-Nitro-propyl)-cyclohexanol (59906-63-7)

Guidance literature:

entspr. Nitronatdianion-Derivat (4), Cyclohexanon;

Reference yield: 81.0%

1-(1-Nitro-propyl)-cyclohexanol (59906-63-7) + acetic anhydride (108-24-7) → 1-(1'-nitropropyl)cyclohexyl acetate

Guidance literature:

With sulfuric acid; at 50 ℃; for 0.333333h;

DOI:10.1080/00397919608003835

upstream raw materials:

cyclohexanone

1-Nitropropane

Downstream raw materials:

1-(1-nitropropyl)cyclohexene

1-(1-aminopropyl)cyclohexanol