1-(1-Ethoxyethenyl)-4-nitrobenzene

Base Information

• Chemical Name: 1-(1-Ethoxyethenyl)-4-nitrobenzene
• CAS No.: 59938-04-4
• Molecular Formula: C10H11NO3
• Molecular Weight: 193.202
• DSSTox Substance ID: DTXSID80496583
• Wikidata: Q82345550

Synonyms:1-(1-Ethoxyethenyl)-4-nitrobenzene;59938-04-4;SCHEMBL10754805;DTXSID80496583

Chemical Property of 1-(1-Ethoxyethenyl)-4-nitrobenzene

Chemical Property:

• XLogP3: 2.7
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 3
• Exact Mass: 193.07389321
• Heavy Atom Count: 14
• Complexity: 214

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCOC(=C)C1=CC=C(C=C1)[N+](=O)[O-]

Technology Process of 1-(1-Ethoxyethenyl)-4-nitrobenzene

There total 4 articles about 1-(1-Ethoxyethenyl)-4-nitrobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

trimethyl(1-ethoxylvinyl)tin (112713-84-5) + para-nitrophenyl bromide (586-78-7) → 4-nitro-1-(1-ethoxyvinyl)benzene (59938-04-4)

Guidance literature:

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; In toluene; at 105 ℃; for 18h;

DOI:10.1021/jo00297a029

Reference yield:

tributyl(1-ethoxyvinyl)stannane (97674-02-7) + para-nitrophenyl bromide (586-78-7) → 4-nitro-1-(1-ethoxyvinyl)benzene (59938-04-4)

Guidance literature:

With bis-triphenylphosphine-palladium(II) chloride; In 1,4-dioxane; at 90 ℃; for 2h;

DOI:10.1016/S0960-894X(03)00258-0

Reference yield:

1-(4-nitro-phenyl)-ethanone-diethylacetal (64600-23-3) → 4-nitro-1-(1-ethoxyvinyl)benzene (59938-04-4)

Guidance literature:

With p-toluenesulfonyl chloride;

DOI:10.1021/jo00398a019

upstream raw materials:

1-(4-nitro-phenyl)-ethanone-diethylacetal

trimethyl(1-ethoxylvinyl)tin

para-nitrophenyl bromide

tributyl(1-ethoxyvinyl)stannane

Downstream raw materials:

1-Ethoxy-1-p-nitrophenyl-2-trichloroacetylethylen

(4-nitrophenyl)ethanone

4-Nitrophenacyl bromide

4-(4-nitrophenyl)oxazole

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