2-Pyrrolidinone, 1-methyl-3-(phenylthio)-

Base Information

Chemical Name:2-Pyrrolidinone, 1-methyl-3-(phenylthio)-
CAS No.:59953-50-3
Molecular Formula:C11H13NOS
Molecular Weight:207.296
Hs Code.:
DSSTox Substance ID:DTXSID30456915
Nikkaji Number:J1.198.800H

Synonyms:59953-50-3;2-Pyrrolidinone, 1-methyl-3-(phenylthio)-;DTXSID30456915;1-Methyl-3-(phenylthio)pyrrolidine-2-one

Suppliers and Price of 2-Pyrrolidinone, 1-methyl-3-(phenylthio)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of 2-Pyrrolidinone, 1-methyl-3-(phenylthio)-

Chemical Property:

XLogP3:2.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:207.07178521
Heavy Atom Count:14
Complexity:213

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CN1CCC(C1=O)SC2=CC=CC=C2

Technology Process of 2-Pyrrolidinone, 1-methyl-3-(phenylthio)-

There total 3 articles about 2-Pyrrolidinone, 1-methyl-3-(phenylthio)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3-diazo-1-methylpyrrolidin-2-one

: 108-98-5
thiophenol

: 59953-50-3
1-methyl-3-phenylsulfanyl-2-pyrrolidinone

Guidance literature:: 3-diazo-1-methylpyrrolidin-2-one; With aluminum oxide; In dichloromethane;

thiophenol; With dirhodium tetraacetate; In dichloromethane; at 20 ℃; for 0.25h;
DOI:10.3762/bjoc.16.55

Reference yield:

: ethyl 2-hydroxy-2-(1-methyl-2-oxopyrrolidin-3-ylidene)acetate

: 59953-50-3
1-methyl-3-phenylsulfanyl-2-pyrrolidinone

Guidance literature:: Multi-step reaction with 2 steps

1.1: 1,8-diazabicyclo[5.4.0]undec-7-ene; p-nitrobenzenesulfonyl azide / dichloromethane / 0.5 h / 0 °C

2.1: aluminum oxide / dichloromethane

2.2: 0.25 h / 20 °C

With p-nitrobenzenesulfonyl azide; aluminum oxide; 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane;
DOI:10.3762/bjoc.16.55