N-(2,4-Dimethylphenyl)benzenecarboximidoyl chloride

Base Information

• Chemical Name: N-(2,4-Dimethylphenyl)benzenecarboximidoyl chloride
• CAS No.: 60065-94-3
• Molecular Formula: C₁₅H₁₄ClN
• Molecular Weight: 243.736
• DSSTox Substance ID: DTXSID60547663
• Nikkaji Number: J450.162D

Synonyms:N-(2,4-Dimethylphenyl)benzenecarboximidoyl chloride;60065-94-3;DTXSID60547663

Chemical Property of N-(2,4-Dimethylphenyl)benzenecarboximidoyl chloride

Chemical Property:

• XLogP3: 5
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 2
• Exact Mass: 243.0814771
• Heavy Atom Count: 17
• Complexity: 268

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC1=CC(=C(C=C1)N=C(C2=CC=CC=C2)Cl)C

Technology Process of N-(2,4-Dimethylphenyl)benzenecarboximidoyl chloride

There total 1 articles about N-(2,4-Dimethylphenyl)benzenecarboximidoyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-(2,4-dimethylphenyl)benzamide (6328-77-4) → N-xylylbenzimidoylchloride (60065-94-3)

Guidance literature:

With phosphorus pentachloride;

Reference yield: 67.0%

N-xylylbenzimidoylchloride (60065-94-3) → benzoic acid-(2,4-dimethyl-6-nitro-anilide) (139765-24-5)

Guidance literature:

With silver nitrate; In acetonitrile; for 0.5h;

Reference yield: 40.0%

2,5-diphosphinohydroquinone (1220997-34-1) + N-xylylbenzimidoylchloride (60065-94-3) → 2,6-dixylylbenzo[1,2-d:4,5-d']bisoxaphosphole (1220997-32-9)

Guidance literature:

In tetrahydrofuran; for 24h; Reflux;

DOI:10.1021/ja1009426

upstream raw materials:

N-(2,4-dimethylphenyl)benzamide

Downstream raw materials:

5-ethyl-3-(2,4-dimethyl-phenyl)-6-methyl-2-phenyl-3H-pyrimidin-4-one

benzoic acid-(2,4-dimethyl-6-nitro-anilide)

N-benzoyl-N-(2,4-dimethyl-phenyl)-anthranilic acid

N-benzoyl-N-(2,4-dimethyl-phenyl)-anthranilic acid methyl ester

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